ALLYL 5-(BROMOMETHYL)ISOXAZOLE-3-CARBOXYLATE

Base Information

Chemical Name:ALLYL 5-(BROMOMETHYL)ISOXAZOLE-3-CARBOXYLATE
CAS No.:833445-84-4
Molecular Formula:C8H8 Br N O3
Molecular Weight:246.06
Hs Code.:2934999090
Mol file:833445-84-4.mol

Synonyms:3-Isoxazolecarboxylicacid, 5-(bromomethyl)-, 2-propenyl ester (9CI)

Suppliers and Price of ALLYL 5-(BROMOMETHYL)ISOXAZOLE-3-CARBOXYLATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
ALLYL-5-(BROMOMETHYL)ISOXAZOLE-3-CARBOXYLATE 95.00%
5MG
$ 503.06

Total 5 raw suppliers

Chemical Property of ALLYL 5-(BROMOMETHYL)ISOXAZOLE-3-CARBOXYLATE

Chemical Property:

PSA：52.33000
LogP:1.91230

Purity/Quality:

99% ^*data from raw suppliers

ALLYL-5-(BROMOMETHYL)ISOXAZOLE-3-CARBOXYLATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ALLYL 5-(BROMOMETHYL)ISOXAZOLE-3-CARBOXYLATE

There total 3 articles about ALLYL 5-(BROMOMETHYL)ISOXAZOLE-3-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 833445-83-3
3-allyloxycarbonyl-5-hydroxymethylisoxazole

: 833445-84-4
3-allyloxycarbonyl-5-bromomethylisoxazole

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In dichloromethane; at -20 ℃; for 0.5h;
DOI:10.1016/j.bmcl.2004.09.092

Reference yield:

: 139297-56-6
5-(hydroxymethyl)-1,2-oxazole-3-carboxylic acid

: 833445-84-4
3-allyloxycarbonyl-5-bromomethylisoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / K₂CO₃ / dimethylformamide / 7 h / 20 °C

2: 56 percent / PPh₃; CBr₄ / CH₂Cl₂ / 0.5 h / -20 °C

With carbon tetrabromide; potassium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2004.09.092

Reference yield:

: 123770-62-7
ethyl 5-(hydroxymethyl)isoxazole-3-carboxylate

: 833445-84-4
3-allyloxycarbonyl-5-bromomethylisoxazole

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / Claisen's alkali / methanol / 0.5 h / 0 °C

2: 76 percent / K₂CO₃ / dimethylformamide / 7 h / 20 °C

3: 56 percent / PPh₃; CBr₄ / CH₂Cl₂ / 0.5 h / -20 °C

With carbon tetrabromide; Claisen's alkali; potassium carbonate; triphenylphosphine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2004.09.092