4,6-O-benzylidene-1,2-dideoxy-3-O-formyl-1-nitro-D-ribo-hex-1-enopyranose

Base Information

Chemical Name:4,6-O-benzylidene-1,2-dideoxy-3-O-formyl-1-nitro-D-ribo-hex-1-enopyranose
CAS No.:117363-34-5
Molecular Formula:C₁₄H₁₃NO₇
Molecular Weight:307.26
Hs Code.:

Synonyms:4,6-O-benzylidene-1,2-dideoxy-3-O-formyl-1-nitro-D-ribo-hex-1-enopyranose

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Chemical Property of 4,6-O-benzylidene-1,2-dideoxy-3-O-formyl-1-nitro-D-ribo-hex-1-enopyranose

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Technology Process of 4,6-O-benzylidene-1,2-dideoxy-3-O-formyl-1-nitro-D-ribo-hex-1-enopyranose

There total 1 articles about 4,6-O-benzylidene-1,2-dideoxy-3-O-formyl-1-nitro-D-ribo-hex-1-enopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 105874-31-5
4,6-O-Benzyliden-1,2-didesoxy-1-nitro-D-arabino-hex-1-enopyranose

: 117363-34-5
4,6-O-benzylidene-1,2-dideoxy-3-O-formyl-1-nitro-D-ribo-hex-1-enopyranose

: (2R,4aR,8aS)-2-phenyl-4,4a-dihydropyrano-[3,2-d][1,3]dioxin-6(8aH)-one

Guidance literature:: With formic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1002/hlca.19880710216

Reference yield: 77.0%

: 117363-34-5
4,6-O-benzylidene-1,2-dideoxy-3-O-formyl-1-nitro-D-ribo-hex-1-enopyranose

: 4,6-O-benzylidene-1,2-dideoxy-1-nitro-D-ribo-hex-1-enopyranose

Guidance literature:: With sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1002/hlca.19880710216

Reference yield:

: 117363-34-5
4,6-O-benzylidene-1,2-dideoxy-3-O-formyl-1-nitro-D-ribo-hex-1-enopyranose

: 2-acetamido-3-azido-4,6-O-benzylidene-1,2,3-trideoxy-1-nitro-α-D-mannopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 25 percent aq. NH₃ / 1.) THF, 0 deg C, then r.t. overnight; 2.) methanol, benzene, r.t. overnight

2: 92 percent / CH₂Cl₂; pyridine / 3 h / -30 - 0 °C

With ammonium hydroxide; In pyridine; dichloromethane;
DOI:10.1002/hlca.19880710216