C₂₆H₄₄O₄

Base Information

Chemical Name:C₂₆H₄₄O₄
CAS No.:1351657-11-8
Molecular Formula:C₂₆H₄₄O₄
Molecular Weight:420.633
Hs Code.:

C<sub>26</sub>H<sub>44</sub>O<sub>4</sub>

Synonyms:C₂₆H₄₄O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₄₄O₄

Chemical Property:

Purity/Quality:

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Technology Process of C₂₆H₄₄O₄

There total 23 articles about C₂₆H₄₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1351657-10-7
C₃₂H₅₈O₄Si

: 1351657-11-8
C₂₆H₄₄O₄

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

: 80657-88-1
(2R,4R)-2-Methyl-4-((4S,5R)-2,2,5-trimethyl-[1,3]dioxan-4-yl)-pentan-1-ol

: 1351657-11-8
C₂₆H₄₄O₄

Guidance literature:: Multi-step reaction with 17 steps

1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

2: sodium hydride / tetrahydrofuran

3: diisobutylaluminium hydride / tetrahydrofuran

4: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

5: pyridine; tributylphosphine

6: dichloromethane

7: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

8: sodium periodate / methanol; water

9: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

10: sodium hydride / tetrahydrofuran

11: aluminum oxide; 20 % Pd(OH)2/C; hydrogen / ethanol

12: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane

13: lithium diisopropyl amide / tetrahydrofuran

14: lithium aluminium tetrahydride / tetrahydrofuran

15: 1H-imidazole / dichloromethane

16: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran

17: tetrabutyl ammonium fluoride / tetrahydrofuran

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; aluminum oxide; sodium periodate; lithium aluminium tetrahydride; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 1: Swern oxidation / 2: Horner-Emmons olefination / 4: Katsuki-Sharpless epoxidation / 9: Pummerer rearrangement / 10: Horner-Emmons olefination;
DOI:10.1016/j.tetlet.2011.10.073

Reference yield:

: 1351656-96-6
C₁₄H₂₆O₄

: 1351657-11-8
C₂₆H₄₄O₄

Guidance literature:: Multi-step reaction with 18 steps

1: diisobutylaluminium hydride / tetrahydrofuran

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane

3: sodium hydride / tetrahydrofuran

4: diisobutylaluminium hydride / tetrahydrofuran

5: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane

6: pyridine; tributylphosphine

7: dichloromethane

8: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide

9: sodium periodate / methanol; water

10: 2,6-dimethylpyridine; trifluoroacetic anhydride / acetonitrile

11: sodium hydride / tetrahydrofuran

12: aluminum oxide; 20 % Pd(OH)2/C; hydrogen / ethanol

13: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane

14: lithium diisopropyl amide / tetrahydrofuran

15: lithium aluminium tetrahydride / tetrahydrofuran

16: 1H-imidazole / dichloromethane

17: tetra-(n-butyl)ammonium iodide; potassium hydride / tetrahydrofuran

18: tetrabutyl ammonium fluoride / tetrahydrofuran

With pyridine; 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; aluminum oxide; sodium periodate; lithium aluminium tetrahydride; oxalyl dichloride; diethyl (2S,3S)-tartrate; tributylphosphine; 20 % Pd(OH)2/C; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium hydride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; lithium diisopropyl amide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 2: Swern oxidation / 3: Horner-Emmons olefination / 5: Katsuki-Sharpless epoxidation / 10: Pummerer rearrangement / 11: Horner-Emmons olefination;
DOI:10.1016/j.tetlet.2011.10.073