(E,E)-p-Divinylbenzene-β,β'-ylene bis(4-tetradecachlorotriphenylmethyl) diradical

Base Information

• Chemical Name: (E,E)-p-Divinylbenzene-β,β'-ylene bis(4-tetradecachlorotriphenylmethyl) diradical
• CAS No.: 329897-46-3
• Molecular Formula: C₄₈H₈Cl₂₈
• Molecular Weight: 1577.28

Synonyms:(E,E)-p-Divinylbenzene-β,β'-ylene bis(4-tetradecachlorotriphenylmethyl) diradical

Chemical Property of (E,E)-p-Divinylbenzene-β,β'-ylene bis(4-tetradecachlorotriphenylmethyl) diradical

Chemical Property:

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Technology Process of (E,E)-p-Divinylbenzene-β,β'-ylene bis(4-tetradecachlorotriphenylmethyl) diradical

There total 1 articles about (E,E)-p-Divinylbenzene-β,β'-ylene bis(4-tetradecachlorotriphenylmethyl) diradical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1-[Bis(2,3,4,5,6-pentachlorophenyl)methyl]-4-{(E)-2-{4-{(E)-2-{4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorophenyl}ethenyl}phenyl}ethenyl}-2,3,5,6-tetrachlorobenzene (329897-51-0) → (E,E)-p-Divinylbenzene-β,β'-ylene bis(4-tetradecachlorotriphenylmethyl) diradical (329897-46-3)

Guidance literature:

1-[Bis(2,3,4,5,6-pentachlorophenyl)methyl]-4-{(E)-2-{4-{(E)-2-{4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorophenyl}ethenyl}phenyl}ethenyl}-2,3,5,6-tetrachlorobenzene; With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; for 1.5h;

With chloranil; In tetrahydrofuran; for 0.5h; Further stages.;

DOI:10.1002/1521-3765(20010105)7:1<240::AID-CHEM240>3.0.CO;2-H

Reference yield:

(E,E)-p-Divinylbenzene-β,β'-ylene bis(4-tetradecachlorotriphenylmethyl) diradical (329897-46-3) → C48H8Cl28(2-)

Guidance literature:

electrochemical reduction;

Reference yield:

(E,E)-p-Divinylbenzene-β,β'-ylene bis(4-tetradecachlorotriphenylmethyl) diradical (329897-46-3) → C48H8Cl28(1-)

Guidance literature:

electrochemical reduction;

upstream raw materials:

1-[Bis(2,3,4,5,6-pentachlorophenyl)methyl]-4-{(E)-2-{4-{(E)-2-{4-[bis(2,3,4,5,6-pentachlorophenyl)methyl]-2,3,5,6-tetrachlorophenyl}ethenyl}phenyl}ethenyl}-2,3,5,6-tetrachlorobenzene

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