1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole

Base Information

Chemical Name:1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole
CAS No.:308248-95-5
Molecular Formula:C₁₅H₁₂F₂N₂O₂
Molecular Weight:290.269
Hs Code.:

Synonyms:1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole

Suppliers and Price of 1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole

There total 3 articles about 1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 308248-90-0
1-(2,4-difluorophenyl)-6,6-dimethyl-4-oxo-4,5,6,7-tetrahydroindazole

: 308248-95-5
1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole

Guidance literature:: With sulfuric acid; selenious acid; In 1,4-dioxane; for 8h; Heating;
DOI:10.1007/BF02269546

Reference yield:

: 40594-29-4,51523-79-6
(2,4-difluorophenyl)hydrazinium chloride

: 308248-95-5
1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂O / 80 - 90 °C

2: 92 percent / conc. HCl / ethanol / 3 h / Heating

3: 85 percent / selenious acid; conc. H₂SO₄ / dioxane / 8 h / Heating

With hydrogenchloride; sulfuric acid; selenious acid; In 1,4-dioxane; ethanol; water; 1: Condensation / 2: Cyclization / 3: Oxidation;
DOI:10.1007/BF02269546

Reference yield:

: 308248-86-4
2-(2,4-difluorophenylhydrazinomethylene)-5,5-dimethyl-1,3-cyclohexandione

: 308248-95-5
1-(2,4-difluorophenyl)-6,6-dimethyl-4,5-dioxo-4,5,6,7-tetrahydroindazole

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / conc. HCl / ethanol / 3 h / Heating

2: 85 percent / selenious acid; conc. H₂SO₄ / dioxane / 8 h / Heating

With hydrogenchloride; sulfuric acid; selenious acid; In 1,4-dioxane; ethanol; 1: Cyclization / 2: Oxidation;
DOI:10.1007/BF02269546