Zn(II) 4'-chloroflavonolate (3,3'-iminobis(N,N-dimethylpropylamine)) perchlorate

Base Information

Chemical Name:Zn(II) 4'-chloroflavonolate (3,3'-iminobis(N,N-dimethylpropylamine)) perchlorate
CAS No.:359643-73-5
Molecular Formula:C₂₅H₃₃ClN₃O₃Zn*ClO₄
Molecular Weight:623.849
Hs Code.:

Synonyms:Zn(II) 4'-chloroflavonolate (3,3'-iminobis(N,N-dimethylpropylamine)) perchlorate

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Chemical Property of Zn(II) 4'-chloroflavonolate (3,3'-iminobis(N,N-dimethylpropylamine)) perchlorate

Chemical Property:

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Technology Process of Zn(II) 4'-chloroflavonolate (3,3'-iminobis(N,N-dimethylpropylamine)) perchlorate

There total 1 articles about Zn(II) 4'-chloroflavonolate (3,3'-iminobis(N,N-dimethylpropylamine)) perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: zinc perchlorate

: 19275-70-8
3-Hydroxy-4'-chloroflavone

: 6711-48-4,86003-72-7
N,N-bis-(3-dimethylaminopropyl)amine

: 359643-73-5
Zn(II) 4'-chloroflavonolate (3,3'-iminobis(N,N-dimethylpropylamine)) perchlorate

Guidance literature:: In ethanol; toluene; (Ar), Zn salt mixed with anine in toluene-ethanol 1:1, stirred for 1 h, treated with flavonol, refluxed for 3 h, cooled to room temp.; filtered, recrystd.(toluene-ethanol 1:1), IR, NMR, UV;
DOI:10.1016/S1381-1169(01)00130-3

Reference yield:

: 359643-73-5
Zn(II) 4'-chloroflavonolate (3,3'-iminobis(N,N-dimethylpropylamine)) perchlorate

: 80937-33-3
oxygen

: [C₆H₄OCO₂COC₆H₄ClZn[(CH₃)2NC₃H₆]2NH]⁽¹⁺⁾*ClO₄^(1-)=[C₆H₄OCO₂COC₆H₄ClZn[(CH₃)2NC₃H₆]2NH]ClO₄

Guidance literature:: In N,N-dimethyl-formamide; byproducts: CO; (Ar), at 100-130°C; not isolated, detected by NMR; Kinetics;
DOI:10.1016/S1381-1169(01)00130-3