1-(4,4'-dimethoxytriphenylmethyloxy)-3-(pyren-2-ylmethylthio)-propan-2-ol

Base Information

• Chemical Name: 1-(4,4'-dimethoxytriphenylmethyloxy)-3-(pyren-2-ylmethylthio)-propan-2-ol
• CAS No.: 753479-91-3
• Molecular Formula: C₄₁H₃₆O₄S
• Molecular Weight: 624.8

Synonyms:1-(4,4'-dimethoxytriphenylmethyloxy)-3-(pyren-2-ylmethylthio)-propan-2-ol

Chemical Property of 1-(4,4'-dimethoxytriphenylmethyloxy)-3-(pyren-2-ylmethylthio)-propan-2-ol

Chemical Property:

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Technology Process of 1-(4,4'-dimethoxytriphenylmethyloxy)-3-(pyren-2-ylmethylthio)-propan-2-ol

There total 2 articles about 1-(4,4'-dimethoxytriphenylmethyloxy)-3-(pyren-2-ylmethylthio)-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

3-(pyren-1-ylmethylthio)-propane-1,2-diol (753479-89-9) + 4,4'-dimethoxytrityl chloride (40615-36-9) → 1-(4,4'-dimethoxytriphenylmethyloxy)-3-(pyren-2-ylmethylthio)-propan-2-ol (753479-91-3)

Guidance literature:

With pyridine; at 20 ℃; for 24h;

DOI:10.1081/NCN-120027829

Reference yield:

1-chloromethylpyrene (1086-00-6) → 1-(4,4'-dimethoxytriphenylmethyloxy)-3-(pyren-2-ylmethylthio)-propan-2-ol (753479-91-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / triethylamine / toluene / 20 h / 20 °C

2: 66 percent / pyridine / 24 h / 20 °C

With pyridine; triethylamine; In toluene;

DOI:10.1081/NCN-120027829

Reference yield: 62.0%

1-(4,4'-dimethoxytriphenylmethyloxy)-3-(pyren-2-ylmethylthio)-propan-2-ol (753479-91-3) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → diisopropyl-phosphoramidous acid 2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-1-(pyren-1-ylmethylsulfanylmethyl)-ethyl ester 2-cyano-ethyl ester

Guidance literature:

With N,N-diisopropylamine tetrazolide; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1081/NCN-120027829

upstream raw materials:

3-(pyren-1-ylmethylthio)-propane-1,2-diol

4,4'-dimethoxytrityl chloride

1-chloromethylpyrene

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