N-(3-methoxy-1-(naphthalen-1-yl)-1H-inden-2-yl)-4-methyl-N-phenylbenzenesulfonamide

Base Information

Chemical Name:N-(3-methoxy-1-(naphthalen-1-yl)-1H-inden-2-yl)-4-methyl-N-phenylbenzenesulfonamide
CAS No.:1638755-64-2
Molecular Formula:C₃₃H₂₇NO₃S
Molecular Weight:517.648
Hs Code.:

Synonyms:N-(3-methoxy-1-(naphthalen-1-yl)-1H-inden-2-yl)-4-methyl-N-phenylbenzenesulfonamide

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Chemical Property of N-(3-methoxy-1-(naphthalen-1-yl)-1H-inden-2-yl)-4-methyl-N-phenylbenzenesulfonamide

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Technology Process of N-(3-methoxy-1-(naphthalen-1-yl)-1H-inden-2-yl)-4-methyl-N-phenylbenzenesulfonamide

There total 7 articles about N-(3-methoxy-1-(naphthalen-1-yl)-1H-inden-2-yl)-4-methyl-N-phenylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1638755-34-6
N-((2-(methoxy(naphthalen-1-yl)methyl)phenyl)ethynyl)-4-methyl-Nphenylbenzenesulfonamide

: 1638755-55-1
N-(2-methoxy-1-(naphthalen-1-yl)-1H-inden-3-yl)-4-methyl-N-phenylbenzenesulfonamide

: 1638755-64-2
N-(3-methoxy-1-(naphthalen-1-yl)-1H-inden-2-yl)-4-methyl-N-phenylbenzenesulfonamide

Guidance literature:: With tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/chem.201403040

Reference yield:

: 380500-63-0
naphthalen-1-yl(2-((trimethylsilyl)ethynyl)phenyl)methanol

: 1638755-64-2
N-(3-methoxy-1-(naphthalen-1-yl)-1H-inden-2-yl)-4-methyl-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / Cooling with ice

1.2: 2 h / 20 °C

2.1: potassium carbonate; methanol / 1 h / 20 °C

3.1: sodium carbonate; copper dichloride; oxygen; pyridine / toluene / 70 °C

3.2: 8 h / 70 °C / 760.05 Torr

4.1: tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate / dichloromethane / 3 h / 20 °C / Inert atmosphere

With pyridine; methanol; tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate; oxygen; sodium hydride; sodium carbonate; potassium carbonate; copper dichloride; In tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1002/chem.201403040

Reference yield:

: 77123-58-1
2-[2-(trimethylsilyl)ethynyl]benzaldehyde

: 1638755-64-2
N-(3-methoxy-1-(naphthalen-1-yl)-1H-inden-2-yl)-4-methyl-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium; iodine

1.2: 1 h / -78 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / Cooling with ice

2.2: 2 h / 20 °C

3.1: potassium carbonate; methanol / 1 h / 20 °C

4.1: sodium carbonate; copper dichloride; oxygen; pyridine / toluene / 70 °C

4.2: 8 h / 70 °C / 760.05 Torr

5.1: tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate / dichloromethane / 3 h / 20 °C / Inert atmosphere

With pyridine; methanol; tris(p-trifluoromethylphenyl)phosphine gold bis(trifluoromethanesulfonyl)imidate; iodine; oxygen; sodium hydride; sodium carbonate; potassium carbonate; magnesium; copper dichloride; In tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1002/chem.201403040