methyl 5-acetamido-2,6-anhydro-9-O-benzyl-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate

Base Information

Chemical Name:methyl 5-acetamido-2,6-anhydro-9-O-benzyl-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate
CAS No.:1314035-79-4
Molecular Formula:C₂₂H₃₁NO₈
Molecular Weight:437.49
Hs Code.:

Synonyms:methyl 5-acetamido-2,6-anhydro-9-O-benzyl-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate

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Chemical Property of methyl 5-acetamido-2,6-anhydro-9-O-benzyl-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate

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Technology Process of methyl 5-acetamido-2,6-anhydro-9-O-benzyl-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate

There total 3 articles about methyl 5-acetamido-2,6-anhydro-9-O-benzyl-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1314035-67-0
methyl 5-acetamido-2,6-anhydro-8,9-O-benzylidene-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate

: 1314035-79-4
methyl 5-acetamido-2,6-anhydro-9-O-benzyl-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate

Guidance literature:: With aluminum (III) chloride; trimethylamine-borane; In tetrahydrofuran; water; at 20 ℃; for 4h;
DOI:10.1039/c0ob01176b

Reference yield:

: 132591-10-7
methyl (2-C-allyl-5-N-acetamido-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulopyranitol)onate

: 1314035-79-4
methyl 5-acetamido-2,6-anhydro-9-O-benzyl-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / acetonitrile / 0 - 20 °C

2: aluminum (III) chloride; trimethylamine-borane / tetrahydrofuran; water / 4 h / 20 °C

With aluminum (III) chloride; trimethylamine-borane; toluene-4-sulfonic acid; In tetrahydrofuran; water; acetonitrile;
DOI:10.1039/c0ob01176b

Reference yield:

: 132591-09-4
(1S,2R)-1-((2R,3R,4S,6R)-3-acetamido-4-acetoxy-6-allyl-6-(methoxycarbonyl)tetrahydro-2H-pyran-2-yl)propane-1,2,3-triyltriacetate

: 1314035-79-4
methyl 5-acetamido-2,6-anhydro-9-O-benzyl-3,5-dideoxy-2-C-(prop-2-enyl)-D-erythro-L-manno-nononate

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; sodium methylate / 20 °C

2: toluene-4-sulfonic acid / acetonitrile / 0 - 20 °C

3: aluminum (III) chloride; trimethylamine-borane / tetrahydrofuran; water / 4 h / 20 °C

With methanol; aluminum (III) chloride; trimethylamine-borane; sodium methylate; toluene-4-sulfonic acid; In tetrahydrofuran; water; acetonitrile;
DOI:10.1039/c0ob01176b