C₅₄H₃₄

Base Information

• Chemical Name: C₅₄H₃₄
• CAS No.: 1158227-53-2
• Molecular Formula: C₅₄H₃₄
• Molecular Weight: 682.864
• Mol file: 1158227-53-2.mol

Synonyms:C₅₄H₃₄

Chemical Property of C₅₄H₃₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₄H₃₄

There total 4 articles about C₅₄H₃₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C34H29BO2 (1158227-50-9) + 2-bromo-9,10-diphenylanthracene (201731-79-5) → C54H34 (1158227-53-2)

Guidance literature:

With Aliquat 336; calcium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; toluene; at 130 ℃; for 4h;

Reference yield:

benzo[l]phenanthrene-2-boronic acid (654664-63-8) → C54H34 (1158227-53-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium carbonate / trans-bis(triphenylphosphine)palladium dichloride / toluene / 3 h / 100 °C

2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 25 °C

3.1: Aliquat 336; calcium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 4 h / 130 °C

With n-butyllithium; Aliquat 336; sodium carbonate; calcium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trans-bis(triphenylphosphine)palladium dichloride; In tetrahydrofuran; hexane; water; toluene;

Reference yield:

C28H17Br (1158227-46-3) → C54H34 (1158227-53-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 25 °C

2.1: Aliquat 336; calcium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 4 h / 130 °C

With n-butyllithium; Aliquat 336; calcium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; water; toluene;

upstream raw materials:

C₃₄H₂₉BO₂

2-bromo-9,10-diphenylanthracene

2-bromobenzo[9,10]phenanthrene

benzo[l]phenanthrene-2-boronic acid