3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium betaine

Base Information

• Chemical Name: 3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium betaine
• CAS No.: 71141-12-3
• Molecular Formula: C₁₇H₁₆N₄S
• Molecular Weight: 308.407

Synonyms:3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium betaine

Chemical Property of 3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium betaine

Chemical Property:

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Technology Process of 3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium betaine

There total 4 articles about 3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium betaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methylbenzothiohydrazide (21048-05-5) → 3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium betaine (71141-12-3)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / Heating

2: NH₃ / CH₂Cl₂

With ammonia; In dichloromethane; benzene;

DOI:10.1039/c39760000439

Reference yield:

3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium; bromide (71141-07-6) → 3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium betaine (71141-12-3)

Guidance literature:

With ammonia; In dichloromethane;

DOI:10.1039/c39760000439

Reference yield:

(4-methyl-benzylidene)-carbonohydrazonic acid dibromide (61199-52-8) → 3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium betaine (71141-12-3)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene / Heating

2: NH₃ / CH₂Cl₂

With ammonia; In dichloromethane; benzene;

DOI:10.1039/c39760000439

upstream raw materials:

3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium; bromide

4-methyl-benzaldehyde (1⁽²⁾H-tetrazol-5-yl)-hydrazone

(4-methyl-benzylidene)-carbonohydrazonic acid dibromide

N-methylbenzothiohydrazide

Downstream raw materials:

3-methyl-5-[(4-methyl-benzylidene)-hydrazino]-2-phenyl-[1,3,4]thiadiazolium; bromide

4-methyl-benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone

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