trans-5,6-dihydroxy-1-phenyl-1-phenyl-2-(N,N-di-n-propyl)aminoindan hydrobromide

Base Information

Chemical Name:trans-5,6-dihydroxy-1-phenyl-1-phenyl-2-(N,N-di-n-propyl)aminoindan hydrobromide
CAS No.:147001-31-8
Molecular Formula:BrH*C₂₁H₂₇NO₂
Molecular Weight:406.363
Hs Code.:

Synonyms:trans-5,6-dihydroxy-1-phenyl-1-phenyl-2-(N,N-di-n-propyl)aminoindan hydrobromide

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Chemical Property of trans-5,6-dihydroxy-1-phenyl-1-phenyl-2-(N,N-di-n-propyl)aminoindan hydrobromide

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Technology Process of trans-5,6-dihydroxy-1-phenyl-1-phenyl-2-(N,N-di-n-propyl)aminoindan hydrobromide

There total 4 articles about trans-5,6-dihydroxy-1-phenyl-1-phenyl-2-(N,N-di-n-propyl)aminoindan hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: ((1S,2S)-5,6-Dimethoxy-1-phenyl-indan-2-yl)-dipropyl-amine

: 147001-31-8
trans-5,6-dihydroxy-1-phenyl-1-phenyl-2-(N,N-di-n-propyl)aminoindan hydrobromide

Guidance literature:: With hydrogen bromide; at 130 ℃; for 3h;
DOI:10.1016/0223-5234(92)90086-G

Reference yield:

: 146655-99-4
5,6-dimethoxy-3-phenyl-2-amino-1-indanone

: 147001-31-8
trans-5,6-dihydroxy-1-phenyl-1-phenyl-2-(N,N-di-n-propyl)aminoindan hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / NaBH₄ / methanol; H₂O / 16 h / Ambient temperature

2: 75 percent / H₂, 35percent aq. HCl / 10percent Pd/C / ethanol / 60 °C / 2068.6 Torr

3: K₂CO₃ / dimethylformamide / 6 h / 65 °C

4: 49 percent / 40percent HBr / 3 h / 130 °C

With hydrogenchloride; sodium tetrahydroborate; hydrogen bromide; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(92)90086-G

Reference yield:

: 146656-00-0
5,6-dimethoxy-3-phenyl-2-amino-1-hydroxy-indan

: 147001-31-8
trans-5,6-dihydroxy-1-phenyl-1-phenyl-2-(N,N-di-n-propyl)aminoindan hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / H₂, 35percent aq. HCl / 10percent Pd/C / ethanol / 60 °C / 2068.6 Torr

2: K₂CO₃ / dimethylformamide / 6 h / 65 °C

3: 49 percent / 40percent HBr / 3 h / 130 °C

With hydrogenchloride; hydrogen bromide; hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(92)90086-G