4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-benzylamide

Base Information

• Chemical Name: 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-benzylamide
• CAS No.: 2836-79-5
• Molecular Formula: C₁₄H₁₄F₃N₃O₄S₂
• Molecular Weight: 409.41

Synonyms:4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-benzylamide

Chemical Property of 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-benzylamide

Chemical Property:

Purity/Quality:

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Technology Process of 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-benzylamide

There total 3 articles about 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-benzyl-1,1,3-trioxo-6-trifluoromethyl-1,2,3,4-tetrahydro-1λ6-benzo[1,2,4]thiadiazine-7-sulfonic acid amide (2250-74-0) → 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-benzylamide (2836-79-5)

Guidance literature:

(alkaline hydrolysis);

DOI:10.1021/jm00325a018

Reference yield:

1,1,3-trioxo-6-trifluoromethyl-1,2,3,4-tetrahydro-1λ6-benzo[1,2,4]thiadiazine-7-sulfonic acid amide (447-82-5) → 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-benzylamide (2836-79-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (benzylation)

2: (alkaline hydrolysis)

DOI:10.1021/jm00325a018

Reference yield:

→ 4-amino-6-trifluoromethyl-benzene-1,3-disulfonic acid 1-amide 3-benzylamide (2836-79-5)

Guidance literature:

aus entspr. Benzothiadiazin;

upstream raw materials:

2-benzyl-1,1,3-trioxo-6-trifluoromethyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-7-sulfonic acid amide

1,1,3-trioxo-6-trifluoromethyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-7-sulfonic acid amide

Downstream raw materials:

2-benzyl-1,1-dioxo-3-(2-oxo-propyl)-6-trifluoromethyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-7-sulfonic acid amide

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