Technology Process of C33H34O9
There total 8 articles about C33H34O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; silver carbonate;
In
toluene;
at 80 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ja200034b
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium diacetate / acetonitrile / 12 h / 24 °C / Inert atmosphere
2.1: tris(diethylamino)sulfonium difluorotrimethylsiliconate / dichloromethane / 0.25 h / -78 °C / Inert atmosphere
2.2: 0.75 h / 24 °C / pH 7 / aq. phosphate buffer
3.1: palladium diacetate; silver carbonate / toluene / 2 h / 80 °C / Inert atmosphere
With
tris(diethylamino)sulfonium difluorotrimethylsiliconate; palladium diacetate; silver carbonate;
In
dichloromethane; toluene; acetonitrile;
DOI:10.1021/ja200034b
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridinium p-toluenesulfonate / acetonitrile / 1.75 h / 24 - 50 °C / Inert atmosphere
1.2: 24 °C / Inert atmosphere
2.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.5 h / -50 - -30 °C / Inert atmosphere
2.2: 1.33 h / -78 - 24 °C / Inert atmosphere
3.1: palladium diacetate / acetonitrile / 12 h / 24 °C / Inert atmosphere
4.1: tris(diethylamino)sulfonium difluorotrimethylsiliconate / dichloromethane / 0.25 h / -78 °C / Inert atmosphere
4.2: 0.75 h / 24 °C / pH 7 / aq. phosphate buffer
5.1: palladium diacetate; silver carbonate / toluene / 2 h / 80 °C / Inert atmosphere
With
copper(l) iodide; tris(diethylamino)sulfonium difluorotrimethylsiliconate; palladium diacetate; pyridinium p-toluenesulfonate; silver carbonate;
In
tetrahydrofuran; diethyl ether; dichloromethane; toluene; acetonitrile;
DOI:10.1021/ja200034b
