3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid

Base Information

• Chemical Name: 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid
• CAS No.: 174406-14-5
• Molecular Formula: C₂₄H₂₉N₅O₉
• Molecular Weight: 531.522

Synonyms:3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid

Chemical Property of 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid

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Technology Process of 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid

There total 1 articles about 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.3%

3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile) (161061-17-2) → 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid (174406-14-5)

Guidance literature:

With hydrogenchloride; water; at 100 ℃; for 2h; Heating / reflux;

Reference yield:

3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid (174406-14-5) → 3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1(15),11,13-triene-6-(2'-methoxy-5'-aminophenyl)methyl-3,6,9-tripotassium acetate

Guidance literature:

3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(2'-methoxy-5'-nitrophenyl)methyl-3,6,9-triacetic acid; With potassium hydroxide; In water; pH=9;

With hydrogen; platinum(IV) oxide; In water; for 1.25h;

upstream raw materials:

3,6,9,15-tetraazabicyclo[9.3.1]pentadeca-1⁽¹⁵⁾,11,13-triene-6-(carboxymethoxy-(2'-methoxy-5'-nitrophenyl)methyl)-3,9-bis(methylenenitrile)

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