(5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-hydroxyethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

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Chemical Name:(5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-hydroxyethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one
CAS No.:1164114-98-0
Molecular Formula:C₄₂H₆₂O₁₀Si
Molecular Weight:755.034
Hs Code.:

(5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-hydroxyethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

Synonyms:(5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-hydroxyethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

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Chemical Property of (5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-hydroxyethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

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Technology Process of (5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-hydroxyethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

There total 1 articles about (5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-hydroxyethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1164115-16-5
C₄₄H₆₈O₁₁Si

: 1164114-98-0
(5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-hydroxyethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

Guidance literature:: With titanium(IV) isopropylate; In benzene; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol900757k

Reference yield: 91.0%

: 1164114-98-0
(5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-hydroxyethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

: 1234579-93-1
(5S,6S)-6-((E)-2-((4R,5R)-2-(2,4-dimethoxyphenyl)-4-(2-azidoethyl)-5-((R)-3-(4-methoxybenzyloxy)-2-(triisopropylsilyloxy)propyl)-1,3-dioxolan-4-yl)vinyl)-5-ethyl-5,6-dihydro-2H-pyran-2-one

Guidance literature:: With zinc azide * 2 pyridine; di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; Inert atmosphere;
DOI:10.1002/chem.201000104