(Z)-phenyl N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propaneselenoimidate

Base Information

Chemical Name:(Z)-phenyl N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propaneselenoimidate
CAS No.:873112-54-0
Molecular Formula:C₂₃H₂₀N₂Se
Molecular Weight:403.385
Hs Code.:

Synonyms:(Z)-phenyl N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propaneselenoimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-phenyl N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propaneselenoimidate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of (Z)-phenyl N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propaneselenoimidate

There total 5 articles about (Z)-phenyl N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propaneselenoimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(2-prop-1-ynyl-phenyl)-2-pyridin-4-yl-propionimidoyl chloride

: 1666-13-3
diphenyl diselenide

: 873112-54-0
(Z)-phenyl N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propaneselenoimidate

Guidance literature:: With potassium tri-sec-butyl-borohydride; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jo0519920

Reference yield:

: 873112-52-8
N-(2-iodophenyl)-2-(pyridin-4-yl)propanamide

: 873112-54-0
(Z)-phenyl N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propaneselenoimidate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / (PPh₃)2PdCl₂; triethylamine; CuI / dimethylformamide / -50 - 20 °C

2: COCl₂; DMF / CH₂Cl₂; toluene / 0 - 20 °C

3: K-selrctride / tetrahydrofuran / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium tri-sec-butyl-borohydride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 1: Sonogashira coupling;
DOI:10.1021/jo0519920

Reference yield:

: 873112-53-9
N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propanamide

: 873112-54-0
(Z)-phenyl N-[2-(prop-1-ynyl)phenyl]-2-(pyridin-4-yl)propaneselenoimidate

Guidance literature:: Multi-step reaction with 2 steps

1: COCl₂; DMF / CH₂Cl₂; toluene / 0 - 20 °C

2: K-selrctride / tetrahydrofuran / 20 °C

With potassium tri-sec-butyl-borohydride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo0519920