1-o-tolyl-1,3-dihydro-benzo[c][1,2]oxaborole

Base Information

• Chemical Name: 1-o-tolyl-1,3-dihydro-benzo[c][1,2]oxaborole
• CAS No.: 96983-87-8
• Molecular Formula: C₁₄H₁₃BO
• Molecular Weight: 208.068
• Mol file: 96983-87-8.mol

Synonyms:1-o-tolyl-1,3-dihydro-benzo[c][1,2]oxaborole

Chemical Property of 1-o-tolyl-1,3-dihydro-benzo[c][1,2]oxaborole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-o-tolyl-1,3-dihydro-benzo[c][1,2]oxaborole

There total 2 articles about 1-o-tolyl-1,3-dihydro-benzo[c][1,2]oxaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ortho-tolylmagnesium bromide (932-31-0) + 3H-benzo[c][1,2]oxaborol-1-ol (5735-41-1) → 1-o-tolyl-1,3-dihydro-benzo[c][1,2]oxaborole (96983-87-8)

Guidance literature:

In diethyl ether; Heating;

DOI:10.1021/jo01034a025

Reference yield:

1,3,1',3'-tetrahydro-1,1'-oxy-bis-benzo[c][1,2]oxaborole (5735-42-2) → 1-o-tolyl-1,3-dihydro-benzo[c][1,2]oxaborole (96983-87-8)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O

2: diethyl ether / Heating

With water; In diethyl ether;

DOI:10.1021/jo01034a025

upstream raw materials:

ortho-tolylmagnesium bromide

3H-benzo[c][1,2]oxaborol-1-ol

1,3,1',3'-tetrahydro-1,1'-oxy-bis-benzo[c][1,2]oxaborole