3-iodo-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-N²-((1-(p-tolyl)-1H-1,2,3-triazol-4-yl)methyl)phthalamide

Base Information

• Chemical Name: 3-iodo-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-N²-((1-(p-tolyl)-1H-1,2,3-triazol-4-yl)methyl)phthalamide
• CAS No.: 1629909-17-6
• Molecular Formula: C₂₈H₂₁F₇IN₅O₂
• Molecular Weight: 719.4

Synonyms:3-iodo-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-N²-((1-(p-tolyl)-1H-1,2,3-triazol-4-yl)methyl)phthalamide

Chemical Property of 3-iodo-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-N²-((1-(p-tolyl)-1H-1,2,3-triazol-4-yl)methyl)phthalamide

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Technology Process of 3-iodo-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-N²-((1-(p-tolyl)-1H-1,2,3-triazol-4-yl)methyl)phthalamide

There total 4 articles about 3-iodo-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-N²-((1-(p-tolyl)-1H-1,2,3-triazol-4-yl)methyl)phthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-iodophthalic anhydride (28418-88-4) → 3-iodo-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-N2-((1-(p-tolyl)-1H-1,2,3-triazol-4-yl)methyl)phthalamide (1629909-17-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: acetonitrile / 20 °C

2.1: trifluoroacetic anhydride / toluene / 0.5 h / 20 °C

2.2: 1 h / Cooling with ice

3.1: copper(l) iodide; triethylamine / 20 °C

With copper(l) iodide; triethylamine; trifluoroacetic anhydride; In toluene; acetonitrile;

DOI:10.1002/cjoc.201400202

Reference yield:

3-iodo-2-(prop-2-yn-1-ylcarbamoyl)benzoic acid (1629909-42-7) → 3-iodo-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-N2-((1-(p-tolyl)-1H-1,2,3-triazol-4-yl)methyl)phthalamide (1629909-17-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic anhydride / toluene / 0.5 h / 20 °C

1.2: 1 h / Cooling with ice

2.1: copper(l) iodide; triethylamine / 20 °C

With copper(l) iodide; triethylamine; trifluoroacetic anhydride; In toluene;

DOI:10.1002/cjoc.201400202

Reference yield:

p-toluidine (106-49-0,12221-03-3) → 3-iodo-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)-N2-((1-(p-tolyl)-1H-1,2,3-triazol-4-yl)methyl)phthalamide (1629909-17-6)

Guidance literature:

Multi-step reaction with 2 steps

1: tert.-butylnitrite; trimethylsilylazide / acetonitrile / 2 h / 0 - 20 °C

2: copper(l) iodide; triethylamine / 20 °C

With copper(l) iodide; tert.-butylnitrite; trimethylsilylazide; triethylamine; In acetonitrile;

DOI:10.1002/cjoc.201400202

upstream raw materials:

3-iodo-2-(prop-2-yn-1-ylcarbamoyl)benzoic acid

3-iodophthalic anhydride

p-toluidine

p-methylazidobenzene

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