1-{4-[2-(4-Acetyl-3-hydroxy-phenyl)-1-ethyl-butyl]-2-hydroxy-phenyl}-ethanone

Base Information

Chemical Name:1-{4-[2-(4-Acetyl-3-hydroxy-phenyl)-1-ethyl-butyl]-2-hydroxy-phenyl}-ethanone
CAS No.:89106-30-9
Molecular Formula:C₂₂H₂₆O₄
Molecular Weight:354.446
Hs Code.:

Synonyms:1-{4-[2-(4-Acetyl-3-hydroxy-phenyl)-1-ethyl-butyl]-2-hydroxy-phenyl}-ethanone

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Chemical Property of 1-{4-[2-(4-Acetyl-3-hydroxy-phenyl)-1-ethyl-butyl]-2-hydroxy-phenyl}-ethanone

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Technology Process of 1-{4-[2-(4-Acetyl-3-hydroxy-phenyl)-1-ethyl-butyl]-2-hydroxy-phenyl}-ethanone

There total 4 articles about 1-{4-[2-(4-Acetyl-3-hydroxy-phenyl)-1-ethyl-butyl]-2-hydroxy-phenyl}-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 89106-31-0
meso-3,4-bis(4-acetyl-3-methoxyphenyl)hexane

: 89106-30-9
1-{4-[2-(4-Acetyl-3-hydroxy-phenyl)-1-ethyl-butyl]-2-hydroxy-phenyl}-ethanone

Guidance literature:: With boron trichloride; In dichloromethane; at -60 ℃; for 0.5h;
DOI:10.1021/jm00371a004

Reference yield:

: 37951-49-8
1-(3-methoxyphenyl)propan-1-one

: 89106-30-9
1-{4-[2-(4-Acetyl-3-hydroxy-phenyl)-1-ethyl-butyl]-2-hydroxy-phenyl}-ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / Zn, TiCl₄ / dioxane / 4 h / 101 °C

2: 95 percent / H₂ / 10percent Pd/C / ethanol

3: 70 percent / AlCl₃ / nitrobenzene / 4 h / Ambient temperature

4: 89 percent / BCl₃ / CH₂Cl₂ / 0.5 h / -60 °C

With aluminium trichloride; hydrogen; boron trichloride; titanium tetrachloride; zinc; palladium on activated charcoal; In 1,4-dioxane; ethanol; dichloromethane; nitrobenzene;
DOI:10.1021/jm00371a004

Reference yield:

: 76473-05-7
C₂₀H₂₄O₂

: 89106-30-9
1-{4-[2-(4-Acetyl-3-hydroxy-phenyl)-1-ethyl-butyl]-2-hydroxy-phenyl}-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂ / 10percent Pd/C / ethanol

2: 70 percent / AlCl₃ / nitrobenzene / 4 h / Ambient temperature

3: 89 percent / BCl₃ / CH₂Cl₂ / 0.5 h / -60 °C

With aluminium trichloride; hydrogen; boron trichloride; palladium on activated charcoal; In ethanol; dichloromethane; nitrobenzene;
DOI:10.1021/jm00371a004