C₂₀H₂₂O₄

Base Information

Chemical Name:C₂₀H₂₂O₄
CAS No.:1282454-89-0
Molecular Formula:C₂₀H₂₂O₄
Molecular Weight:326.392
Hs Code.:

C<sub>20</sub>H<sub>22</sub>O<sub>4</sub>

Synonyms:C₂₀H₂₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₂O₄

Chemical Property:

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Technology Process of C₂₀H₂₂O₄

There total 1 articles about C₂₀H₂₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 670-80-4
4-cyclohexen-1-ylmorpholine

: 100-20-9
terephthaloyl chloride

: 1282454-89-0
C₂₀H₂₂O₄

Guidance literature:: 4-cyclohexen-1-ylmorpholine; terephthaloyl chloride; With trimethylamine; In 1,3,5-trimethyl-benzene; at 35 ℃; for 3h;

With hydrogenchloride; water; for 5h; Reflux;
DOI:10.1039/c0ob00683a

Reference yield: 100.0%

: 1282454-89-0
C₂₀H₂₂O₄

: C₂₁H₂₆O₆^(2-)*2Na⁽¹⁺⁾

Guidance literature:: With sodium hydroxide; In ethanol; for 1h; Reflux;
DOI:10.1039/c0ob00683a

Reference yield:

: 1282454-89-0
C₂₀H₂₂O₄

: 1282454-16-3
C₇₂H₈₄O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / ethanol / 1 h / Reflux

2.1: triethanolamine; hydrazine / 4 h / Reflux

2.2: 11 h / 200 - 220 °C

3.1: 1 h / Reflux; Acidic conditions

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / Reflux

5.1: 1H-imidazole / tetrahydrofuran / 2 h / 20 °C

6.1: manganese triacetate / acetic acid / 0.83 h / Inert atmosphere; Sonication

With 1H-imidazole; lithium aluminium tetrahydride; triethanolamine; manganese triacetate; sodium hydroxide; hydrazine; In tetrahydrofuran; ethanol; acetic acid; 2.1: Wolff-Kishner reduction;
DOI:10.1039/c0ob00683a