Technology Process of benzyl-[1-(2-(cyclohex-1-enyl)ethyl)butyl]amine
There total 9 articles about benzyl-[1-(2-(cyclohex-1-enyl)ethyl)butyl]amine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
benzylamine; 1-(cyclohex-1-enyl)hexan-3-one;
With
toluene-4-sulfonic acid;
In
benzene;
for 8h;
Heating;
With
sodium tetrahydroborate;
In
ethanol;
at 20 ℃;
for 1h;
DOI:10.1081/SCC-120037916
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 70 percent / BH3*Me2S / tetrahydrofuran / 10 h / 20 °C
2.1: CH2Cl2 / 1.5 h / 20 °C
3.1: SOCl2; pyridine / 0.25 h / -15 °C
4.1: 1.34 g / KOH; H2O / methanol / 1 h
5.1: PCC / CH2Cl2 / 1 h / 20 °C
6.1: 85 percent / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C
7.1: 100 percent / CrO3; pyridine / CH2Cl2 / 0.25 h / 20 °C
8.1: p-toluenesulfonic acid / benzene / 8 h / Heating
8.2: 80 percent / NaBH4 / ethanol / 1 h / 20 °C
With
pyridine; chromium(VI) oxide; potassium hydroxide; thionyl chloride; dimethylsulfide borane complex; water; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; benzene;
DOI:10.1081/SCC-120037916
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: PCC / CH2Cl2 / 1 h / 20 °C
2.1: 85 percent / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C
3.1: 100 percent / CrO3; pyridine / CH2Cl2 / 0.25 h / 20 °C
4.1: p-toluenesulfonic acid / benzene / 8 h / Heating
4.2: 80 percent / NaBH4 / ethanol / 1 h / 20 °C
With
pyridine; chromium(VI) oxide; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
tetrahydrofuran; diethyl ether; dichloromethane; benzene;
DOI:10.1081/SCC-120037916