benzoic acid (3S,4R)-bis-(tert-butyl-dimethyl-silanyloxy)-5-oxo-heptyl ester

Base Information

Chemical Name:benzoic acid (3S,4R)-bis-(tert-butyl-dimethyl-silanyloxy)-5-oxo-heptyl ester
CAS No.:1103963-19-4
Molecular Formula:C₂₆H₄₆O₅Si₂
Molecular Weight:494.819
Hs Code.:

Synonyms:benzoic acid (3S,4R)-bis-(tert-butyl-dimethyl-silanyloxy)-5-oxo-heptyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzoic acid (3S,4R)-bis-(tert-butyl-dimethyl-silanyloxy)-5-oxo-heptyl ester

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Technology Process of benzoic acid (3S,4R)-bis-(tert-butyl-dimethyl-silanyloxy)-5-oxo-heptyl ester

There total 1 articles about benzoic acid (3S,4R)-bis-(tert-butyl-dimethyl-silanyloxy)-5-oxo-heptyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1103963-55-8
benzoic acid-(3S,4R)-dihydroxy-5-oxo-heptyl ester

: 69739-34-0
t-butyldimethylsiyl triflate

: 1103963-19-4
benzoic acid (3S,4R)-bis-(tert-butyl-dimethyl-silanyloxy)-5-oxo-heptyl ester

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -78 - 20 ℃; for 1h;
DOI:10.1002/anie.200803271

Reference yield: 88.0%

: 1103963-19-4
benzoic acid (3S,4R)-bis-(tert-butyl-dimethyl-silanyloxy)-5-oxo-heptyl ester

: 2,4-Dimethylhexa-2,4-dienal

: 1103963-34-3
C₃₄H₅₈O₆Si₂

Guidance literature:: benzoic acid (3S,4R)-bis-(tert-butyl-dimethyl-silanyloxy)-5-oxo-heptyl ester; With titanium tetrachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 3.5h;

2,4-Dimethylhexa-2,4-dienal; In dichloromethane; at -78 - -35 ℃;

With water; ammonium chloride; at 0 - 20 ℃; optical yield given as %de;
DOI:10.1002/anie.200803271