C₄₇H₆₆O₈Si

Base Information

Chemical Name:C₄₇H₆₆O₈Si
CAS No.:155154-03-3
Molecular Formula:C₄₇H₆₆O₈Si
Molecular Weight:787.122
Hs Code.:

C<sub>47</sub>H<sub>66</sub>O<sub>8</sub>Si

Synonyms:C₄₇H₆₆O₈Si

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Chemical Property of C₄₇H₆₆O₈Si

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Technology Process of C₄₇H₆₆O₈Si

There total 13 articles about C₄₇H₆₆O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 155005-79-1
C₄₇H₆₅BrO₈Si

: C₄₇H₆₆O₈Si

: 155154-03-3
C₄₇H₆₆O₈Si

Guidance literature:: With triphenylstannane; In benzene; at 50 ℃; for 2h;
DOI:10.1021/ja00081a050

Reference yield: 10.0%

: 155005-79-1
C₄₇H₆₅BrO₈Si

: C₄₇H₆₄O₈Si

: C₄₇H₆₆O₈Si

: 155154-03-3
C₄₇H₆₆O₈Si

Guidance literature:: With tri-n-butyl-tin hydride; at 80 ℃;
DOI:10.1021/ja00081a050

Reference yield:

: C₂₉H₄₆O₅

: 155154-03-3
C₄₇H₆₆O₈Si

Guidance literature:: Multi-step reaction with 11 steps

1: 90 percent / DMAP, Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

2: 1.) Py*HCl, (Cl₂CHCO)2O, 2.) Na₂CO₃ / 1.) xylene, 150-155 deg C, 0.5 h, 2.) acetone, H₂O, 25 deg C, 14 h

3: pyridine / 5 h / 0 °C

4: 1.) PhSeSePh, NaBH₄, 2.) mCPBA, Na₂CO₃ / 1.) EtOH, reflux, 1.5 h, 2.) THF, 25 deg C, 24 h

5: MeSOPh / CH₂Cl₂ / -78 °C

6: 94 percent / thiourea, NaHCO₃ / ethanol / 18 h / 70 °C

7: 85 percent / ClCH₂CO₂H, DEAD, PPh₃ / 18 h / 25 °C

8: 99 percent / AgNO₃ / dimethylformamide / 0.08 h / 25 °C

9: 1.) OsO₄, (S,S)-N,N-di<(mesitylene)methyl>-1,2-diphenyl-1,2-ethylenediamine, 2.) aq. NaHSO₃ / 1.) CH₂Cl₂, -100 deg C, 0.5 h, 2.) THF, reflux

10: 91 percent / NBS / tetrahydrofuran / 0.5 h / -78 °C

11: n-Bu₃SnH / 80 °C

With pyridine; dmap; sodium tetrahydroborate; N-Bromosuccinimide; osmium(VIII) oxide; racemic methyl phenyl sulfoxide; diphenyl diselenide; tri-n-butyl-tin hydride; pyridine hydrochloride; sodium hydrogencarbonate; sodium carbonate; silver nitrate; sodium hydrogensulfite; dichloroacetic anhydride; (1S,2S)-1,2-diphenyl-N¹,N²-bis(mesitylmethyl)ethane-1,2-diamine; triethylamine; thiourea; chloroacetic acid; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00081a050