2-{4-[4-(1-hydroxy-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester

Base Information

Chemical Name:2-{4-[4-(1-hydroxy-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester
CAS No.:937021-10-8
Molecular Formula:C₁₉H₂₇N₃O₅
Molecular Weight:377.44
Hs Code.:

Synonyms:2-{4-[4-(1-hydroxy-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester

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Chemical Property of 2-{4-[4-(1-hydroxy-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester

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Technology Process of 2-{4-[4-(1-hydroxy-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester

There total 11 articles about 2-{4-[4-(1-hydroxy-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 937021-07-3
2-(4-azidobutoxy)benzoic acid 2-methoxyethyl ester

: 115-19-5
2-methyl-but-3-yn-2-ol

: 937021-10-8
2-{4-[4-(1-hydroxy-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 25 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201001677

Reference yield: 5.0%

: 937021-08-4
benzylcarbamic acid 1,1-dimethylprop-2-ynyl ester

: 937021-07-3
2-(4-azidobutoxy)benzoic acid 2-methoxyethyl ester

: 937021-09-5
C₂₇H₃₄N₄O₆

: 937021-10-8
2-{4-[4-(1-hydroxy-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester

: 2-{4-[4-(1-benzylamino-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester

: 2-[4-(4-isoprenyl-[1,2,3]triazol-1-yl)-butoxy]-benzoic acid 2-methoxyethyl ester

Guidance literature:: With L-ascorbic acid sodium salt; copper(II) sulfate; In water; tert-butyl alcohol; at 20 ℃;
DOI:10.1021/jo070131j

Reference yield:

: 937021-08-4
benzylcarbamic acid 1,1-dimethylprop-2-ynyl ester

: 937021-07-3
2-(4-azidobutoxy)benzoic acid 2-methoxyethyl ester

: 937021-10-8
2-{4-[4-(1-hydroxy-1-methyl-ethyl)-[1,2,3]triazol-1-yl]-butoxy}-benzoic acid 2-methoxyethyl ester

: 100-46-9
benzylamine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; copper(l) iodide / 24 h / 20 °C

2: acetonitrile / pH 4.3 / aq. buffer

With pyridine; copper(l) iodide; In acetonitrile; 1: Huisgen cycloaddition;
DOI:10.1016/j.tet.2010.11.026