(S)-benzoic acid 2-sec-butylphenyl ester

Base Information

Chemical Name:(S)-benzoic acid 2-sec-butylphenyl ester
CAS No.:1286745-33-2
Molecular Formula:C₁₇H₁₈O₂
Molecular Weight:254.329
Hs Code.:

Synonyms:(S)-benzoic acid 2-sec-butylphenyl ester

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Chemical Property of (S)-benzoic acid 2-sec-butylphenyl ester

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Technology Process of (S)-benzoic acid 2-sec-butylphenyl ester

There total 7 articles about (S)-benzoic acid 2-sec-butylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1286745-32-1
(S)-benzoic acid 2-(3-iodo-1-methylpropyl)phenyl ester

: 1286745-33-2
(S)-benzoic acid 2-sec-butylphenyl ester

Guidance literature:: (S)-benzoic acid 2-(3-iodo-1-methylpropyl)phenyl ester; With 2,2'-azobis(isobutyronitrile); In benzene; for 0.5h; Inert atmosphere;

With tri-n-butyl-tin hydride; In benzene; at 70 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja110052n

Reference yield:

: 1286745-31-0
(S)-benzoic acid 2-(3-hydroxy-1-methylpropyl)phenyl ester

: 1286745-33-2
(S)-benzoic acid 2-sec-butylphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran; acetonitrile / 0.75 h / 20 °C / Inert atmosphere

2.1: 2,2'-azobis(isobutyronitrile) / benzene / 0.5 h / Inert atmosphere

2.2: 3 h / 70 °C / Inert atmosphere

With 1H-imidazole; 2,2'-azobis(isobutyronitrile); iodine; triphenylphosphine; In tetrahydrofuran; acetonitrile; benzene;
DOI:10.1021/ja110052n

Reference yield:

: 30825-54-8
(S)-3,4-dihydro-4-methylcoumarin

: 1286745-33-2
(S)-benzoic acid 2-sec-butylphenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere

3.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran; acetonitrile / 0.75 h / 20 °C / Inert atmosphere

4.1: 2,2'-azobis(isobutyronitrile) / benzene / 0.5 h / Inert atmosphere

4.2: 3 h / 70 °C / Inert atmosphere

With 1H-imidazole; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); iodine; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; acetonitrile; benzene;
DOI:10.1021/ja110052n