allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

Base Information

Chemical Name:allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside
CAS No.:874904-99-1
Molecular Formula:C₄₉H₅₁NO₂₁
Molecular Weight:989.938
Hs Code.:

allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

Synonyms:allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

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Chemical Property of allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

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Technology Process of allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

There total 2 articles about allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 874904-93-5
C₃₄H₃₃F₃N₂O₁₄

: 154391-03-4
allyl 2,3-di-O-benzoyl-α-D-galactopyranoside

: 874904-99-1
allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; propiononitrile; at -78 ℃; diastereoselective reaction; Microfluidic conditions;
DOI:10.1021/op900084f

Reference yield:

: 874904-93-5
C₃₄H₃₃F₃N₂O₁₄

: 154391-03-4
allyl 2,3-di-O-benzoyl-α-D-galactopyranoside

: 874904-99-1
allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

: C₄₉H₅₁NO₂₁

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃;
DOI:10.1080/07328300701634796

Reference yield: 84.0%

: 874904-99-1
allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

: 108-24-7
acetic anhydride

: allyl 4-O-acetyl-2,3-di-O-benzoyl-6-O-(methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside

Guidance literature:: allyl 2,3-di-O-benzoyl-6-O-(methyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-5-phthalimido-D-glycero-α-D-galacto-2-nonulopyranosylonate)-α-D-galactopyranoside; With acetic acid; methylhydrazine; In ethanol; at 80 ℃; for 24h;

acetic anhydride; With pyridine; Further stages.;
DOI:10.1080/07328300701634796