N'-[1-amino-3-(phenylsulfanyl)propylid-1-ene]-3-phenylthiopropanehydrazonamide

Base Information

• Chemical Name: N'-[1-amino-3-(phenylsulfanyl)propylid-1-ene]-3-phenylthiopropanehydrazonamide
• CAS No.: 1158839-61-2
• Molecular Formula: C₁₈H₂₂N₄S₂
• Molecular Weight: 358.531

Synonyms:N'-[1-amino-3-(phenylsulfanyl)propylid-1-ene]-3-phenylthiopropanehydrazonamide

Chemical Property of N'-[1-amino-3-(phenylsulfanyl)propylid-1-ene]-3-phenylthiopropanehydrazonamide

Chemical Property:

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Technology Process of N'-[1-amino-3-(phenylsulfanyl)propylid-1-ene]-3-phenylthiopropanehydrazonamide

There total 2 articles about N'-[1-amino-3-(phenylsulfanyl)propylid-1-ene]-3-phenylthiopropanehydrazonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

3-(phenylthio)propanimidic acid ethyl ester hydrochloride → 3,6-bis(2-phenylsulfanylethyl)-1,2,4,5-tetrazine (1158839-64-5) + N'-[1-amino-3-(phenylsulfanyl)propylid-1-ene]-3-phenylthiopropanehydrazonamide (1158839-61-2)

Guidance literature:

With hydrazine hydrate; triethylamine; In ethanol; at -10 - 20 ℃; Inert atmosphere;

DOI:10.1055/s-0028-1087818

Reference yield:

3-(phenylthio)propanimidic acid ethyl ester hydrochloride → 3,6-bis(2-phenylsulfanylethyl)-1,2,4,5-tetrazine (1158839-64-5) + N'-[1-amino-3-(phenylsulfanyl)propylid-1-ene]-3-phenylthiopropanehydrazonamide (1158839-61-2) + 4-amino-3,5-bis(2-phenylsulfanylethyl)-1,2,4-triazole (1158839-63-4) + 3,6-bis-(2-phenylsulfanylethyl)-1,2-dihydro-1,2,4,5-tetrazine (1158839-62-3)

Guidance literature:

With hydrazine hydrate; triethylamine; In ethanol; at -10 - 20 ℃; Inert atmosphere;

DOI:10.1055/s-0028-1087818

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