ethyl 2-{[(cyclohexylamino)carbonyl]amino}-4,5-dimethyl-3-thiophenecarboxylate

Base Information

Chemical Name:ethyl 2-{[(cyclohexylamino)carbonyl]amino}-4,5-dimethyl-3-thiophenecarboxylate
CAS No.:203808-30-4
Molecular Formula:C₁₆H₂₄N₂O₃S
Molecular Weight:324.444
Hs Code.:
Mol file:203808-30-4.mol

Synonyms:2-(3-Cyclohexyl-ureido)-4,5-dimethyl-thiophene-3-carboxylic acid ethyl ester

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Chemical Property of ethyl 2-{[(cyclohexylamino)carbonyl]amino}-4,5-dimethyl-3-thiophenecarboxylate

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Technology Process of ethyl 2-{[(cyclohexylamino)carbonyl]amino}-4,5-dimethyl-3-thiophenecarboxylate

There total 1 articles about ethyl 2-{[(cyclohexylamino)carbonyl]amino}-4,5-dimethyl-3-thiophenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 3173-53-3
Cyclohexyl isocyanate

: 4815-24-1
2-amino-4,5-dimethyl-3-thiophenecarboxylic acid ethyl ester

: 203808-30-4
2-(3-Cyclohexyl-ureido)-4,5-dimethyl-thiophene-3-carboxylic acid ethyl ester

Guidance literature:: In toluene; for 8h; Heating;

Reference yield: 98.0%

: 203808-30-4
2-(3-Cyclohexyl-ureido)-4,5-dimethyl-thiophene-3-carboxylic acid ethyl ester

: 203808-33-7
3-Cyclohexyl-5,6-dimethyl-1H-thieno[2,3-d]pyrimidine-2,4-dione

Guidance literature:: With potassium hydroxide; In ethanol; water; for 0.5h; Heating; 2.) acidified with glacial acetic acid;

Reference yield:

: 203808-30-4
2-(3-Cyclohexyl-ureido)-4,5-dimethyl-thiophene-3-carboxylic acid ethyl ester

: 203808-39-3
1-Benzyl-3-cyclohexyl-5,6-dimethyl-1H-thieno[2,3-d]pyrimidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / KOH / ethanol; H₂O / 0.5 h / Heating; 2.) acidified with glacial acetic acid

2: 92 percent / NaH 80percent, dispersion in mineral oil / dimethylformamide / 1.) room temp. for 20 min; 2.) room temp. for 4 ds

With potassium hydroxide; dispersion in mineral oil; sodium hydride; In ethanol; water; N,N-dimethyl-formamide;