N-benzhydryl-4-chlorobenzenesulfonamide

Base Information

• Chemical Name: N-benzhydryl-4-chlorobenzenesulfonamide
• CAS No.: 853-84-9
• Molecular Formula: C₁₉H₁₆ClNO₂S
• Molecular Weight: 357.861
• Mol file: 853-84-9.mol

Synonyms:N-p-chlorophenylsulfonyl diphenylmethylamine

Chemical Property of N-benzhydryl-4-chlorobenzenesulfonamide

Chemical Property:

Purity/Quality:

N-BENZHYDRYL-4-CHLORO-BENZENESULFONAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzhydryl-4-chlorobenzenesulfonamide

There total 5 articles about N-benzhydryl-4-chlorobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-Chlorobenzenesulfonamide (98-64-6) + 1,1-Diphenylmethanol (91-01-0) → N-p-chlorophenylsulfonyl diphenylmethylamine (853-84-9)

Guidance literature:

With Bromodiphenylmethane; In neat (no solvent); at 130 ℃; for 24h; Sealed tube; Green chemistry;

DOI:10.1039/c6gc00938g

Reference yield: 97.0%

4-Chlorobenzenesulfonamide (98-64-6) + Diphenylmethane (101-81-5) → N-p-chlorophenylsulfonyl diphenylmethylamine (853-84-9)

Guidance literature:

With [bis(acetoxy)iodo]benzene; iodine; at 50 ℃; Inert atmosphere;

DOI:10.1021/ol900090f

Reference yield: 95.0%

N-benzylidene-4-chlorobenzenesulfonamide (13707-45-4) + sodium tetraphenyl borate (143-66-8) → N-p-chlorophenylsulfonyl diphenylmethylamine (853-84-9)

Guidance literature:

With bis(acetonitrile)(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; 1,4-di(diphenylphosphino)-butane; In 1,4-dioxane; at 90 ℃; for 16h;

DOI:10.1016/S0022-328X(99)00562-8

upstream raw materials:

N-benzylidene-4-chlorobenzenesulfonamide

sodium tetraphenyl borate

4-Chlorobenzenesulfonamide

Diphenylmethane