1-methoxy-2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidine-4-one

Base Information

Chemical Name:1-methoxy-2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidine-4-one
CAS No.:1309689-61-9
Molecular Formula:C₂₃H₂₆N₂O₃S
Molecular Weight:410.537
Hs Code.:

Synonyms:1-methoxy-2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidine-4-one

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Chemical Property of 1-methoxy-2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidine-4-one

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Technology Process of 1-methoxy-2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidine-4-one

There total 4 articles about 1-methoxy-2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidine-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1309689-60-8
2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-4-oxo-2,6,6-trimethylpiperidin-1-oxyl

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 1309689-61-9
1-methoxy-2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidine-4-one

Guidance literature:: With ferrous(II) sulfate heptahydrate; dihydrogen peroxide; In water; at 20 ℃; for 1.5h;
DOI:10.1039/c0cc05764a

Reference yield:

: 5554-54-1
1,2,2,6,6-pentamethyl-4-piperidone

: 1309689-61-9
1-methoxy-2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidine-4-one

Guidance literature:: Multi-step reaction with 4 steps

1: N-benzyl-trimethylammonium hydroxide; ammonium chloride / methanol; dimethyl sulfoxide / 5 h / 20 - 50 °C

2: tri-tert-butyl phosphine; palladium diacetate; caesium carbonate; copper(I) bromide / N,N-dimethyl-formamide / 3 h / 150 °C / Inert atmosphere

3: sodium tungstate (VI) dihydrate; dihydrogen peroxide / methanol; water / 48 h / 20 °C

4: ferrous(II) sulfate heptahydrate; dihydrogen peroxide / water / 1.5 h / 20 °C

With ferrous(II) sulfate heptahydrate; sodium tungstate (VI) dihydrate; tri-tert-butyl phosphine; dihydrogen peroxide; palladium diacetate; N-benzyl-trimethylammonium hydroxide; ammonium chloride; caesium carbonate; copper(I) bromide; In methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1039/c0cc05764a

Reference yield:

: 1309689-58-4
2-(4-bromophenyl)-2,6,6-trimethylpiperidin-4-one

: 1309689-61-9
1-methoxy-2-(4-(6-methoxybenzo[d]thiazol-2-yl)phenyl)-2,6,6-trimethylpiperidine-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: tri-tert-butyl phosphine; palladium diacetate; caesium carbonate; copper(I) bromide / N,N-dimethyl-formamide / 3 h / 150 °C / Inert atmosphere

2: sodium tungstate (VI) dihydrate; dihydrogen peroxide / methanol; water / 48 h / 20 °C

3: ferrous(II) sulfate heptahydrate; dihydrogen peroxide / water / 1.5 h / 20 °C

With ferrous(II) sulfate heptahydrate; sodium tungstate (VI) dihydrate; tri-tert-butyl phosphine; dihydrogen peroxide; palladium diacetate; caesium carbonate; copper(I) bromide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c0cc05764a