1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzothiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine

Base Information

Chemical Name:1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzothiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine
CAS No.:70932-07-9
Molecular Formula:C₂₉H₃₂F₂N₂S₂
Molecular Weight:510.715
Hs Code.:

1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzo<b,f>thiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine

Synonyms:1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzothiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine

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Chemical Property of 1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzothiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine

Chemical Property:

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Technology Process of 1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzothiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine

There total 5 articles about 1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzothiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 371-42-6
4-Fluorothiophenol

: 1-[2-(4-fluorophenylthio)ethyl]piperazino dimaleate hemihydrate

: 1-(2-chloroethyl)-4-(ethoxycarbonyl)piperazino hydrochloride

: 70931-43-0
1-ethoxycarbonyl-4-<2-(4-fluorophenylthio)ethyl>piperazine

: 110-16-7,26099-09-2
maleic acid

: 70932-07-9
1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzothiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine

Guidance literature:: With potassium hydroxide; sodium hydroxide; potassium carbonate; In ethanol; water; acetone;

Reference yield:

: 70932-06-8
1-[4-(3-Fluoro-8-isopropyl-10,11-dihydro-dibenzo[b,f]thiepin-10-yl)-piperazin-1-yl]-2-(4-fluoro-phenylsulfanyl)-ethanone

: 70932-07-9
1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzothiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Yield given;

Reference yield:

: 371-42-6
4-Fluorothiophenol

: 70932-07-9
1-(7-fluorophenyl-2-isopropyl-10,11-dihydrodibenzothiepin-11-yl)-4-(2-(4-fluorophenylthio)ethyl)piperazine

Guidance literature:: Multi-step reaction with 4 steps

1: 53 percent / NaOH / aq. ethanol / 2 h / Heating

2: 88 percent / SOCl₂ / 2 h / Heating

3: CHCl₃ / Ambient temperature; overnight

4: LiAlH₄ / diethyl ether

With sodium hydroxide; lithium aluminium tetrahydride; thionyl chloride; In diethyl ether; ethanol; chloroform;