3,4-dimethyl-1-phenyl-1H-phosphole-2-carbaldehyde tungsten

Base Information

Chemical Name:3,4-dimethyl-1-phenyl-1H-phosphole-2-carbaldehyde tungsten
CAS No.:146687-56-1
Molecular Formula:C₁₈H₁₃O₆PW
Molecular Weight:540.121
Hs Code.:

Synonyms:3,4-dimethyl-1-phenyl-1H-phosphole-2-carbaldehyde tungsten

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Chemical Property of 3,4-dimethyl-1-phenyl-1H-phosphole-2-carbaldehyde tungsten

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Technology Process of 3,4-dimethyl-1-phenyl-1H-phosphole-2-carbaldehyde tungsten

There total 3 articles about 3,4-dimethyl-1-phenyl-1H-phosphole-2-carbaldehyde tungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: C₂₄H₁₅O₁₁PW₂

: 146687-56-1
3,4-dimethyl-1-phenyl-1H-phosphole-2-carbaldehyde tungsten

Guidance literature:: With water; In toluene; at 90 ℃; Inert atmosphere; Sealed tube;
DOI:10.1021/om400109h

Reference yield:

: 146440-99-5
1-phenyl-2-bromo-3,4-dimethylphosphole

: 146687-56-1
3,4-dimethyl-1-phenyl-1H-phosphole-2-carbaldehyde tungsten

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -100 - -90 °C / Inert atmosphere

1.2: 0.5 h / -90 °C / Inert atmosphere

2.1: tetrahydrofuran; hexane / 20 °C / Inert atmosphere

3.1: water / toluene / 90 °C / Inert atmosphere; Sealed tube

With n-butyllithium; water; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/om400109h

Reference yield:

: 14040-11-0
tungsten hexacarbonyl

: 146687-56-1
3,4-dimethyl-1-phenyl-1H-phosphole-2-carbaldehyde tungsten

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -100 - -90 °C / Inert atmosphere

1.2: 0.5 h / -90 °C / Inert atmosphere

2.1: tetrahydrofuran; hexane / 20 °C / Inert atmosphere

3.1: water / toluene / 90 °C / Inert atmosphere; Sealed tube

With n-butyllithium; water; In tetrahydrofuran; hexane; toluene;
DOI:10.1021/om400109h