1,3-Bis(4-isopropylphenyl)cyclopentaphenanthren-2-one

Base Information

• Chemical Name: 1,3-Bis(4-isopropylphenyl)cyclopentaphenanthren-2-one
• CAS No.: 108868-47-9
• Molecular Formula: C₃₅H₃₀O
• Molecular Weight: 466.623

Synonyms:1,3-Bis(4-isopropylphenyl)cyclopentaphenanthren-2-one

Chemical Property of 1,3-Bis(4-isopropylphenyl)cyclopentaphenanthren-2-one

Chemical Property:

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Technology Process of 1,3-Bis(4-isopropylphenyl)cyclopentaphenanthren-2-one

There total 2 articles about 1,3-Bis(4-isopropylphenyl)cyclopentaphenanthren-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

9,10-phenanthrenequinone (84-11-7) + 1,3-Di-(4-isopropylphenyl)-acetone (108868-48-0) → 1,3-Bis(4-isopropylphenyl)cyclopentaphenanthren-2-one (108868-47-9)

Guidance literature:

With potassium hydroxide; In ethanol; Heating;

DOI:10.1021/ja00249a032

Reference yield:

(4-isopropylphenyl)acetic acid (4476-28-2) → 1,3-Bis(4-isopropylphenyl)cyclopentaphenanthren-2-one (108868-47-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 23 percent / pyridine / acetic anhydride / 6 h / Heating

2: 40 percent / KOH / ethanol / Heating

With pyridine; potassium hydroxide; In ethanol; acetic anhydride;

DOI:10.1021/ja00249a032

Reference yield: 0.9%

9-bromophenanthrene (573-17-1) + 1,3-Bis(4-isopropylphenyl)cyclopentaphenanthren-2-one (108868-47-9) → 9,18-Bis(4-isopropylphenyl)tetrabenzanthracene

Guidance literature:

at 340 ℃; for 4h;

DOI:10.1021/ja00249a032

upstream raw materials:

9,10-phenanthrenequinone

1,3-Di-(4-isopropylphenyl)-acetone

(4-isopropylphenyl)acetic acid

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