N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide

Base Information

Chemical Name:N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide
CAS No.:154653-36-8
Molecular Formula:C₃₂H₃₇N₃O₆
Molecular Weight:559.662
Hs Code.:

Synonyms:N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide

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Chemical Property of N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide

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Technology Process of N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide

There total 4 articles about N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 3789-59-1
(R)-1-phenylpropylamine

: 96188-33-9
N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid

: 154653-36-8
N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide

Guidance literature:: With N-hydroxy-5-norbornene-2,3-dicarboximide; dicyclohexyl-carbodiimide; In 1,4-dioxane; Ambient temperature;
DOI:10.1021/jf00056a003

Reference yield:

: 3479-47-8
Z-Asp(OBzl)-OH

: 154653-36-8
N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide / tetrahydrofuran / Ambient temperature

2: 57 percent / Et₃N / dioxane; H₂O / Ambient temperature

3: 88 percent / dicyclohexylcarbodiimide, N-hydroxy-5-norbornene-2,3-dicarboximide / dioxane / Ambient temperature

With N-hydroxy-5-norbornene-2,3-dicarboximide; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jf00056a003

Reference yield:

: 2941-20-0
1-phenylpropylamine

: 154653-36-8
N-(carbobenzyloxy)-β-benzyl-L-aspartyl-D-α-aminobutyric acid (S)-α-ethylbenzylamide

Guidance literature:: Multi-step reaction with 2 steps

2: 88 percent / dicyclohexylcarbodiimide, N-hydroxy-5-norbornene-2,3-dicarboximide / dioxane / Ambient temperature

With N-hydroxy-5-norbornene-2,3-dicarboximide; dicyclohexyl-carbodiimide; In 1,4-dioxane;
DOI:10.1021/jf00056a003