1-(4,4'-dimethoxydiphenylmethylene)-3-oxo-1,2-diazetidinium hydroxide, inner salt

Base Information

Chemical Name:1-(4,4'-dimethoxydiphenylmethylene)-3-oxo-1,2-diazetidinium hydroxide, inner salt
CAS No.:79289-40-0
Molecular Formula:C₁₇H₁₆N₂O₃
Molecular Weight:296.326
Hs Code.:

Synonyms:1-(4,4'-dimethoxydiphenylmethylene)-3-oxo-1,2-diazetidinium hydroxide, inner salt

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Chemical Property of 1-(4,4'-dimethoxydiphenylmethylene)-3-oxo-1,2-diazetidinium hydroxide, inner salt

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Technology Process of 1-(4,4'-dimethoxydiphenylmethylene)-3-oxo-1,2-diazetidinium hydroxide, inner salt

There total 2 articles about 1-(4,4'-dimethoxydiphenylmethylene)-3-oxo-1,2-diazetidinium hydroxide, inner salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 79289-16-0
4,4'-dimethoxybenzophenone α-chloroacetylhydrazone

: 79289-40-0
1-(4,4'-dimethoxydiphenylmethylene)-3-oxo-1,2-diazetidinium hydroxide, inner salt

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1021/ja00416a009

Reference yield:

: 20114-55-0
4,4'-dimethoxybenzophenone hydrazone

: 79289-40-0
1-(4,4'-dimethoxydiphenylmethylene)-3-oxo-1,2-diazetidinium hydroxide, inner salt

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / pyridine / CH₂Cl₂ / 0.25 h / Heating

2: 70 percent / 53percent sodium hydride / tetrahydrofuran / 24 h / Ambient temperature

With pyridine; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00416a009