C₃₉H₄₂N₂O₆Si

Base Information

Chemical Name:C₃₉H₄₂N₂O₆Si
CAS No.:1093849-16-1
Molecular Formula:C₃₉H₄₂N₂O₆Si
Molecular Weight:662.858
Hs Code.:

C<sub>39</sub>H<sub>42</sub>N<sub>2</sub>O<sub>6</sub>Si

Synonyms:C₃₉H₄₂N₂O₆Si

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Chemical Property of C₃₉H₄₂N₂O₆Si

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Technology Process of C₃₉H₄₂N₂O₆Si

There total 15 articles about C₃₉H₄₂N₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₉H₄₃ClHgN₂O₇Si

: 1093849-16-1
C₃₉H₄₂N₂O₆Si

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In tetrachloromethane; toluene; at 20 - 50 ℃; for 3h;

Reference yield:

: 956485-06-6
3-O-(2-naphthylmethyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 1093849-16-1
C₃₉H₄₂N₂O₆Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane / 1.5 h / 20 °C

3.1: sodium hydroxide / water; tetrahydrofuran / 48 h / 20 °C / Cooling with ice

4.1: triethylamine / 16 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.2: 0.25 h / -78 °C

6.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / Cooling with ice

6.2: 1.5 h / -78 °C

7.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

7.2: 0.25 h / -78 °C

8.1: cerium(III) chloride / tetrahydrofuran / 1.75 h / Cooling with ice

8.2: 1.5 h / -78 °C

9.1: thionyl chloride; pyridine / 1 h / 60 °C

10.1: sulfuric acid / water / 1 h / 20 °C

11.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C

11.2: 4 h / 0 - 70 °C

12.1: ammonia; methanol / 12 h

13.1: dichloromethane / 16 h / 20 °C

13.2: 0.25 h

14.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene; tetrachloromethane / 3 h / 20 - 50 °C

With pyridine; methanol; sodium periodate; thionyl chloride; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); sulfuric acid; ammonia; tri-n-butyl-tin hydride; acetic acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; dichloromethane; water; toluene; acetonitrile; 5.1: Swern Oxidation / 5.2: Swern Oxidation / 7.1: Swern Oxidation / 7.2: Swern Oxidation;

Reference yield:

: 939-26-4
2-bromomethylnaphthyl bromide

: 1093849-16-1
C₃₉H₄₂N₂O₆Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

1.2: 2 h

2.1: acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane / 1.5 h / 20 °C

4.1: sodium hydroxide / water; tetrahydrofuran / 48 h / 20 °C / Cooling with ice

5.1: triethylamine / 16 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 0.25 h / -78 °C

7.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / Cooling with ice

7.2: 1.5 h / -78 °C

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

8.2: 0.25 h / -78 °C

9.1: cerium(III) chloride / tetrahydrofuran / 1.75 h / Cooling with ice

9.2: 1.5 h / -78 °C

10.1: thionyl chloride; pyridine / 1 h / 60 °C

11.1: sulfuric acid / water / 1 h / 20 °C

12.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C

12.2: 4 h / 0 - 70 °C

13.1: ammonia; methanol / 12 h

14.1: dichloromethane / 16 h / 20 °C

14.2: 0.25 h

15.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene; tetrachloromethane / 3 h / 20 - 50 °C

With pyridine; methanol; sodium periodate; thionyl chloride; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); sulfuric acid; ammonia; tri-n-butyl-tin hydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 6.1: Swern Oxidation / 6.2: Swern Oxidation / 8.1: Swern Oxidation / 8.2: Swern Oxidation;