C₂₆H₂₄FNO₃S

Base Information

Chemical Name:C₂₆H₂₄FNO₃S
CAS No.:1381787-07-0
Molecular Formula:C₂₆H₂₄FNO₃S
Molecular Weight:449.546
Hs Code.:

C<sub>26</sub>H<sub>24</sub>FNO<sub>3</sub>S

Synonyms:C₂₆H₂₄FNO₃S

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Chemical Property of C₂₆H₂₄FNO₃S

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Technology Process of C₂₆H₂₄FNO₃S

There total 4 articles about C₂₆H₂₄FNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.3%

: 1381787-06-9
C₁₉H₁₈FNO

: 98-59-9
p-toluenesulfonyl chloride

: 1381787-07-0
C₂₆H₂₄FNO₃S

Guidance literature:: With dmap; In pyridine; at 20 ℃; for 12h; Inert atmosphere;

Reference yield:

: 5332-25-2
6-bromoquinoline

: 1381787-07-0
C₂₆H₂₄FNO₃S

Guidance literature:: Multi-step reaction with 6 steps

1: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 12 h / 0 - 20 °C

2: triethylamine / acetonitrile / 12 h / 20 °C / Inert atmosphere

3: copper(I) bromide / toluene; diethyl ether / 0.5 h / 0 - 20 °C / Inert atmosphere

4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 4 h / 90 °C / Inert atmosphere

5: sodium tetrahydroborate; methanol / 4 h / 0 - 20 °C / Inert atmosphere

6: dmap / pyridine / 12 h / 20 °C / Inert atmosphere

With methanol; dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; triethylamine; 3-chloro-benzenecarboperoxoic acid; copper(I) bromide; In 1,4-dioxane; pyridine; diethyl ether; ethyl acetate; toluene; acetonitrile;

Reference yield:

: 65185-41-3
6-bromoquinoline-2-carbonitrile

: 1381787-07-0
C₂₆H₂₄FNO₃S

Guidance literature:: Multi-step reaction with 4 steps

1: copper(I) bromide / toluene; diethyl ether / 0.5 h / 0 - 20 °C / Inert atmosphere

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 4 h / 90 °C / Inert atmosphere

3: sodium tetrahydroborate; methanol / 4 h / 0 - 20 °C / Inert atmosphere

4: dmap / pyridine / 12 h / 20 °C / Inert atmosphere

With methanol; dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; copper(I) bromide; In 1,4-dioxane; pyridine; diethyl ether; toluene;