ethyl 3-cyclohexyl-2-(2'-thiopyridyl)-2-trifluoroacetoxy propanoate

Base Information

Chemical Name:ethyl 3-cyclohexyl-2-(2'-thiopyridyl)-2-trifluoroacetoxy propanoate
CAS No.:145144-84-9
Molecular Formula:C₁₈H₂₂F₃NO₄S
Molecular Weight:405.438
Hs Code.:

Synonyms:ethyl 3-cyclohexyl-2-(2'-thiopyridyl)-2-trifluoroacetoxy propanoate

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Chemical Property of ethyl 3-cyclohexyl-2-(2'-thiopyridyl)-2-trifluoroacetoxy propanoate

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Technology Process of ethyl 3-cyclohexyl-2-(2'-thiopyridyl)-2-trifluoroacetoxy propanoate

There total 6 articles about ethyl 3-cyclohexyl-2-(2'-thiopyridyl)-2-trifluoroacetoxy propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 368-28-5
ethyl α-(trifluoroacetoxy)acrylate

: 105398-69-4
Cyclohexanecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester

: 145144-84-9
ethyl 3-cyclohexyl-2-(2'-thiopyridyl)-2-trifluoroacetoxy propanoate

Guidance literature:: In dichloromethane; at 0 - 5 ℃; Irradiation;
DOI:10.1016/S0040-4039(00)61177-2

Reference yield:

: 617-35-6
2-oxo-propionic acid ethyl ester

: 145144-84-9
ethyl 3-cyclohexyl-2-(2'-thiopyridyl)-2-trifluoroacetoxy propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / triethylamine / CH₂Cl₂ / 1.) 0 deg C, 2.) room temperature, 2 h

2: 94 percent Spectr_. / 0 °C / Irradiation

With triethylamine; In dichloromethane;
DOI:10.1016/0040-4039(93)88090-6

Reference yield:

: 105398-69-4
Cyclohexanecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester

: 145144-84-9
ethyl 3-cyclohexyl-2-(2'-thiopyridyl)-2-trifluoroacetoxy propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / CH₂Cl₂ / 0 - 5 °C / Irradiation

2: MCPBA

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1016/S0040-4039(00)61177-2