Technology Process of 1-(3,5-Bis-phenyl)-3-pentanone
There total 5 articles about 1-(3,5-Bis-phenyl)-3-pentanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
for 1h;
DOI:10.1055/s-1980-29193
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 91 percent / K2CO3 / acetonitrile / 1.) ice temp, 1 h
2: 95 percent / LiAlH4 / diethyl ether / Heating
3: 88 percent / Pyridinium chlorochromate, CH3COONa / CH2Cl2 / 2 h / 24 - 25 °C
4: 95 percent / NaOH / H2O / 1.) 65 deg C - 70 deg C, 3 h, 2.) 25 deg C
5: 96 percent / H2 / 10percent Pd-C / ethanol / 1 h
With
sodium hydroxide; lithium aluminium tetrahydride; hydrogen; sodium acetate; potassium carbonate; pyridinium chlorochromate;
palladium on activated charcoal;
In
diethyl ether; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1055/s-1980-29193
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 88 percent / Pyridinium chlorochromate, CH3COONa / CH2Cl2 / 2 h / 24 - 25 °C
2: 95 percent / NaOH / H2O / 1.) 65 deg C - 70 deg C, 3 h, 2.) 25 deg C
3: 96 percent / H2 / 10percent Pd-C / ethanol / 1 h
With
sodium hydroxide; hydrogen; sodium acetate; pyridinium chlorochromate;
palladium on activated charcoal;
In
ethanol; dichloromethane; water;
DOI:10.1055/s-1980-29193
