Technology Process of C41H45N5O6Si
There total 9 articles about C41H45N5O6Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C41H46N2O7Si;
With
pyridine; trifluoromethylsulfonic anhydride;
In
dichloromethane;
for 1h;
Inert atmosphere;
Cooling with ice;
With
sodium azide;
In
N,N-dimethyl-formamide;
for 48h;
Inert atmosphere;
- Guidance literature:
-
With
sodium azide;
In
N,N-dimethyl-formamide;
for 48h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: dmap; triethylamine / dichloromethane / 20 h / Inert atmosphere; Cooling; Reflux
2: sulfuric acid; acetic acid / 3.5 h
3: N,O-bis-(trimethylsilyl)-acetamide; trimethylsilyl trifluoromethanesulfonate / acetonitrile / 1 h / 20 °C / Inert atmosphere; Reflux
4: methylamine / water; tetrahydrofuran / 0.5 h / 20 °C
5: dmap; trifluoromethane sulfonyl chloride / dichloromethane / 1 h / 20 °C / Inert atmosphere; Cooling with ice
6: sodium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C
7: pyridine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice
8: sodium azide / N,N-dimethyl-formamide / 48 h / Inert atmosphere
With
pyridine; dmap; sodium azide; N,O-bis-(trimethylsilyl)-acetamide; trifluoromethane sulfonyl chloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; water; acetic acid; triethylamine; methylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
