(E)-(2S,3R)-2-(4-benzyloxy)phenyl-5-(2-methoxycarbonyl)ethenyl-3-methoxycarbonyl-2,3-di-hydrobenzofuran

Base Information

Chemical Name:(E)-(2S,3R)-2-(4-benzyloxy)phenyl-5-(2-methoxycarbonyl)ethenyl-3-methoxycarbonyl-2,3-di-hydrobenzofuran
CAS No.:1042431-35-5
Molecular Formula:C₂₇H₂₄O₆
Molecular Weight:444.484
Hs Code.:

Synonyms:(E)-(2S,3R)-2-(4-benzyloxy)phenyl-5-(2-methoxycarbonyl)ethenyl-3-methoxycarbonyl-2,3-di-hydrobenzofuran

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Chemical Property of (E)-(2S,3R)-2-(4-benzyloxy)phenyl-5-(2-methoxycarbonyl)ethenyl-3-methoxycarbonyl-2,3-di-hydrobenzofuran

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Technology Process of (E)-(2S,3R)-2-(4-benzyloxy)phenyl-5-(2-methoxycarbonyl)ethenyl-3-methoxycarbonyl-2,3-di-hydrobenzofuran

There total 1 articles about (E)-(2S,3R)-2-(4-benzyloxy)phenyl-5-(2-methoxycarbonyl)ethenyl-3-methoxycarbonyl-2,3-di-hydrobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.4%

: 616898-40-9
(2S,3R)-methyl 2-(4-(benzyloxy)phenyl)-5-bromo-2,3-dihydrobenzofuran-3-carboxylate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1042431-35-5
(E)-(2S,3R)-2-(4-benzyloxy)phenyl-5-(2-methoxycarbonyl)ethenyl-3-methoxycarbonyl-2,3-di-hydrobenzofuran

Guidance literature:: With triethylamine; palladium diacetate; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; at 100 ℃; for 24h; Inert atmosphere;

Reference yield: 54.4%

: 1042431-35-5
(E)-(2S,3R)-2-(4-benzyloxy)phenyl-5-(2-methoxycarbonyl)ethenyl-3-methoxycarbonyl-2,3-di-hydrobenzofuran

: 959714-40-0
(R,R)-dehydrodi-p-coumaric acid

Guidance literature:: (E)-(2S,3R)-2-(4-benzyloxy)phenyl-5-(2-methoxycarbonyl)ethenyl-3-methoxycarbonyl-2,3-di-hydrobenzofuran; With lithium hydroxide monohydrate; water; In tetrahydrofuran; methanol; at 20 ℃; for 2h;

With citric acid; In tetrahydrofuran; methanol; water;