C₃₅H₅₂O₆S₂

Base Information

Chemical Name:C₃₅H₅₂O₆S₂
CAS No.:930803-73-9
Molecular Formula:C₃₅H₅₂O₆S₂
Molecular Weight:632.926
Hs Code.:

C<sub>35</sub>H<sub>52</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₃₅H₅₂O₆S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₅H₅₂O₆S₂

Chemical Property:

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Technology Process of C₃₅H₅₂O₆S₂

There total 20 articles about C₃₅H₅₂O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 930803-36-4
C₃₅H₅₀O₆S₂

: 930803-73-9
C₃₅H₅₂O₆S₂

Guidance literature:: With zinc(II) tetrahydroborate; In diethyl ether; at -20 ℃; for 2h;
DOI:10.1002/anie.200604053

Reference yield:

: 930803-26-2
C₉H₁₅S₂OBr

: 930803-73-9
C₃₅H₅₂O₆S₂

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

2: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

3: 80 percent / tert-butyllithium / tetrahydrofuran / -96 - -78 °C

4: 83 percent / Zn(BH₄)2 / diethyl ether / 2 h / -20 °C

With dmap; zinc(II) tetrahydroborate; tert.-butyl lithium; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; lithium bromide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200604053

Reference yield:

: C₇H₁₂OS₂

: 930803-73-9
C₃₅H₅₂O₆S₂

Guidance literature:: Multi-step reaction with 6 steps

1: potassium bis(trimethylsilyl)amide; [18]crown-6; bromine / tetrahydrofuran

2: 99 percent / diisobutylaluminum hydride / CH₂Cl₂ / -45 °C

3: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

4: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

5: 80 percent / tert-butyllithium / tetrahydrofuran / -96 - -78 °C

6: 83 percent / Zn(BH₄)2 / diethyl ether / 2 h / -20 °C

With dmap; zinc(II) tetrahydroborate; 18-crown-6 ether; bromine; tert.-butyl lithium; potassium hexamethylsilazane; diisobutylaluminium hydride; lithium triethylborohydride; methanesulfonyl chloride; triethylamine; lithium bromide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; 1: Horner-Wadsworth-Emmons reaction;
DOI:10.1002/anie.200604053