N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-N-2-propen-1-ylbenzenesulfonamide

Base Information

Chemical Name:N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-N-2-propen-1-ylbenzenesulfonamide
CAS No.:1228430-43-0
Molecular Formula:C₃₁H₃₉NO₃SSi
Molecular Weight:533.807
Hs Code.:

Synonyms:N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-N-2-propen-1-ylbenzenesulfonamide

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Chemical Property of N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-N-2-propen-1-ylbenzenesulfonamide

Chemical Property:

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Technology Process of N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-N-2-propen-1-ylbenzenesulfonamide

There total 1 articles about N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-N-2-propen-1-ylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228430-42-9
N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-benzenesulfonamide

: 106-95-6
allyl bromide

: 1228430-43-0
N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-N-2-propen-1-ylbenzenesulfonamide

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1228430-43-0
N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-N-2-propen-1-ylbenzenesulfonamide

: 1228430-40-7
(2S)-2-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-1-[(4-methylphenyl)sulfonyl]-1,2,3,6-tetrahydropyridine

Guidance literature:: Grubbs catalyst first generation; In dichloromethane; at 20 ℃; Product distribution / selectivity;

Reference yield:

: 1228430-43-0
N-[(1S)-1-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-buten-1-yl]-4-methyl-N-2-propen-1-ylbenzenesulfonamide

: 1228430-41-8
(1R,4S,6R)-4-({[(1,1-dimethylethyl)(diphenyl)silyl]oxy}methyl)-3-[(4-methylphenyl)sulfonyl]-3-azabicyclo[4.1.0]heptane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Grubbs catalyst first generation / dichloromethane / 20 °C

2.1: trifluoroacetic acid; diethylzinc / dichloromethane; hexanes / 0.33 h / 0 °C

2.2: 0 - 20 °C

With diethylzinc; trifluoroacetic acid; Grubbs catalyst first generation; In hexanes; dichloromethane;