(1S,2S)-1-carbomethoxy-1,2-dimethylcyclohexane

Base Information

Chemical Name:(1S,2S)-1-carbomethoxy-1,2-dimethylcyclohexane
CAS No.:139894-33-0
Molecular Formula:C₁₀H₁₈O₂
Molecular Weight:170.252
Hs Code.:

Synonyms:(1S,2S)-1-carbomethoxy-1,2-dimethylcyclohexane

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Chemical Property of (1S,2S)-1-carbomethoxy-1,2-dimethylcyclohexane

Chemical Property:

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Technology Process of (1S,2S)-1-carbomethoxy-1,2-dimethylcyclohexane

There total 5 articles about (1S,2S)-1-carbomethoxy-1,2-dimethylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1S)-6-carbomethoxy-1,6-dimethylcyclohex-1-ene

: 139894-33-0
(1S,2S)-1-carbomethoxy-1,2-dimethylcyclohexane

Guidance literature:: With hydrogen; (η4-1,5-cyclooctadiene)(pyridine)(tricyclohexylphosphine)iridium(I) hexafluorophosphate; In dichloromethane; for 12h; under 760 Torr; Yield given;

Reference yield:

: (1S,6R)-1,6-Dimethyl-5-oxo-cyclohex-3-enecarboxylic acid methyl ester

: 139894-33-0
(1S,2S)-1-carbomethoxy-1,2-dimethylcyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / 5percent Rh/Al₂O₃ / ethyl acetate / 3 h / 760 Torr

2: 97 percent / NaBH₄ / ethanol / 2 h / 0 °C

3: P₂O₅, Celite / benzene / 18 h

4: H₂ / 3>PF₆ / CH₂Cl₂ / 12 h / 760 Torr

With sodium tetrahydroborate; Celite; hydrogen; phosphorus pentoxide; Rh/Al₂O₃; (η4-1,5-cyclooctadiene)(pyridine)(tricyclohexylphosphine)iridium(I) hexafluorophosphate; In ethanol; dichloromethane; ethyl acetate; benzene;

Reference yield:

: 139760-69-3
(1S,2R,3S)-3-carbomethoxy-2,3-dimethyl-1-hydroxycyclohexane

: 139894-33-0
(1S,2S)-1-carbomethoxy-1,2-dimethylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: P₂O₅, Celite / benzene / 18 h

2: H₂ / 3>PF₆ / CH₂Cl₂ / 12 h / 760 Torr

With Celite; hydrogen; phosphorus pentoxide; (η4-1,5-cyclooctadiene)(pyridine)(tricyclohexylphosphine)iridium(I) hexafluorophosphate; In dichloromethane; benzene;