2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)acetaldehyde

Base Information

Chemical Name:2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)acetaldehyde
CAS No.:1262750-11-7
Molecular Formula:C₁₆H₂₂O₅
Molecular Weight:294.348
Hs Code.:

Synonyms:2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)acetaldehyde

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Chemical Property of 2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)acetaldehyde

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Technology Process of 2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)acetaldehyde

There total 8 articles about 2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)ethan-1-ol

: 1262750-11-7
2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)acetaldehyde

Guidance literature:: With sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.5h; Schlenk technique;
DOI:10.1021/acs.orglett.0c03957

Reference yield: 90.0%

: 1262750-10-6
C₃₀H₃₆O₄S₂

: 1262750-11-7
2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)acetaldehyde

Guidance literature:: With iodine; sodium hydrogencarbonate; In water; acetone; at 0 ℃; for 2h;
DOI:10.1021/ja108906e

Reference yield:

: 1013632-80-8
(4R,5R)-4-allyl-5-((4-methoxybenzyloxy)methyl)-2,2-dimethyl-1,3-dioxolane

: 1262750-11-7
2-((4R,5R)-5-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)acetaldehyde

: C₁₆H₂₂O₅

Guidance literature:: With oxygen; copper(l) chloride; palladium dichloride; In water; N,N-dimethyl-formamide; at 20 - 25 ℃; for 75h; under 760.051 Torr; regioselective reaction;
DOI:10.1021/ja108906e