(4R,5S)-(+)-1-[2'-(diphenylmethyleneamino)acetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone

Base Information

Chemical Name:(4R,5S)-(+)-1-[2'-(diphenylmethyleneamino)acetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone
CAS No.:307304-38-7
Molecular Formula:C₂₆H₂₅N₃O₂
Molecular Weight:411.503
Hs Code.:

Synonyms:(4R,5S)-(+)-1-[2'-(diphenylmethyleneamino)acetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5S)-(+)-1-[2'-(diphenylmethyleneamino)acetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone

Chemical Property:

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Technology Process of (4R,5S)-(+)-1-[2'-(diphenylmethyleneamino)acetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone

There total 4 articles about (4R,5S)-(+)-1-[2'-(diphenylmethyleneamino)acetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112791-04-5
(4R,5S)-3,4-dimethyl-5-phenyl-imidazolidin-2-one

: 307304-38-7
(4R,5S)-(+)-1-[2'-(diphenylmethyleneamino)acetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 4 h / 80 °C

2: NaN₃ / acetonitrile / 72 h / 80 °C

3: H₂; HCl / Pd/C / methanol; H₂O

4: CH₂Cl₂ / 24 h / 20 °C

With hydrogenchloride; sodium azide; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; water; acetonitrile; 1: Substitution / 2: Substitution / 3: Catalytic hydrogenation / 4: Condensation;
DOI:10.1021/jo000321t

Reference yield:

: 143359-25-5
(4R,5S)-(+)-(2'-chloroacetyl)-3,4-dimethyl-5-phenyl-2-imidazolidinone

: 307304-38-7
(4R,5S)-(+)-1-[2'-(diphenylmethyleneamino)acetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / acetonitrile / 72 h / 80 °C

2: H₂; HCl / Pd/C / methanol; H₂O

3: CH₂Cl₂ / 24 h / 20 °C

With hydrogenchloride; sodium azide; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; water; acetonitrile; 1: Substitution / 2: Catalytic hydrogenation / 3: Condensation;
DOI:10.1021/jo000321t

Reference yield:

: (4R,5S)-(+)-1-(2'-azidoacetyl)-3,4-dimethyl-5-phenyl-2-imidazolidinone

: 307304-38-7
(4R,5S)-(+)-1-[2'-(diphenylmethyleneamino)acetyl]-3,4-dimethyl-5-phenyl-2-imidazolidinone

Guidance literature:: Multi-step reaction with 2 steps

1: H₂; HCl / Pd/C / methanol; H₂O

2: CH₂Cl₂ / 24 h / 20 °C

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; water; 1: Catalytic hydrogenation / 2: Condensation;
DOI:10.1021/jo000321t