(R)-3-(2-(benzyloxy)-5-methylphenyl)-N,N-di(isopropyl-d7)-3-phenylpropanamide

Base Information

Chemical Name:(R)-3-(2-(benzyloxy)-5-methylphenyl)-N,N-di(isopropyl-d7)-3-phenylpropanamide
CAS No.:1191280-46-2
Molecular Formula:C₂₉H₃₅NO₂
Molecular Weight:443.491
Hs Code.:

Synonyms:(R)-3-(2-(benzyloxy)-5-methylphenyl)-N,N-di(isopropyl-d7)-3-phenylpropanamide

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Chemical Property of (R)-3-(2-(benzyloxy)-5-methylphenyl)-N,N-di(isopropyl-d7)-3-phenylpropanamide

Chemical Property:

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Technology Process of (R)-3-(2-(benzyloxy)-5-methylphenyl)-N,N-di(isopropyl-d7)-3-phenylpropanamide

There total 6 articles about (R)-3-(2-(benzyloxy)-5-methylphenyl)-N,N-di(isopropyl-d7)-3-phenylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1191280-45-1
(R)-3-(2-(benzyloxy)-5-methylphenyl)-3-phenylpropanoyl chloride

: 70237-41-1
bis-(1,2,2,2-tetradeuterio-1-trideuteriomethyl-ethyl)-amine

: 1191280-46-2
(R)-3-(2-(benzyloxy)-5-methylphenyl)-N,N-di(isopropyl-d7)-3-phenylpropanamide

Guidance literature:: (R)-3-(2-(benzyloxy)-5-methylphenyl)-3-phenylpropanoyl chloride; bis-(1,2,2,2-tetradeuterio-1-trideuteriomethyl-ethyl)-amine; With triethylamine; In diethyl ether; for 4h;

With hydrogenchloride; In diethyl ether; water;

Reference yield:

: 6627-55-0
2-bromo-p-cresol

: 1191280-46-2
(R)-3-(2-(benzyloxy)-5-methylphenyl)-N,N-di(isopropyl-d7)-3-phenylpropanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetone / 4 h / Reflux

2.1: iodine; magnesium / tetrahydrofuran / 1 h / 80 °C

2.2: 1 h / -30 °C

2.3: -30 - 20 °C

3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 4 h / 20 °C

3.2: pH 2

4.1: pyridine; thionyl chloride / toluene / 1 h / Reflux

5.1: triethylamine / diethyl ether / 4 h

With pyridine; thionyl chloride; dihydrogen peroxide; iodine; potassium carbonate; magnesium; triethylamine; lithium hydroxide; In tetrahydrofuran; diethyl ether; water; acetone; toluene;

Reference yield:

: 2830-53-7
1-(benzyloxy)-2-bromo-4-methylbenzene

: 1191280-46-2
(R)-3-(2-(benzyloxy)-5-methylphenyl)-N,N-di(isopropyl-d7)-3-phenylpropanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: iodine; magnesium / tetrahydrofuran / 1 h / 80 °C

1.2: 1 h / -30 °C

1.3: -30 - 20 °C

2.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 4 h / 20 °C

2.2: pH 2

3.1: pyridine; thionyl chloride / toluene / 1 h / Reflux

4.1: triethylamine / diethyl ether / 4 h

With pyridine; thionyl chloride; dihydrogen peroxide; iodine; magnesium; triethylamine; lithium hydroxide; In tetrahydrofuran; diethyl ether; water; toluene;