9-Methyl-2-(p-tolylthio)acridine-1,4-dione

Base Information

Chemical Name:9-Methyl-2-(p-tolylthio)acridine-1,4-dione
CAS No.:226260-32-8
Molecular Formula:C₂₁H₁₅NO₂S
Molecular Weight:345.422
Hs Code.:
DSSTox Substance ID:DTXSID901221745
Nikkaji Number:J1.124.911F

Synonyms:9-methyl-2-(4-tolylthio)-1,4-dihydroacridine-1,4-dione;9-methyl-TTDAD

Suppliers and Price of 9-Methyl-2-(p-tolylthio)acridine-1,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 9-Methyl-2-(p-tolylthio)acridine-1,4-dione

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:345.08234989
Heavy Atom Count:25
Complexity:578

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)SC2=CC(=O)C3=NC4=CC=CC=C4C(=C3C2=O)C

Technology Process of 9-Methyl-2-(p-tolylthio)acridine-1,4-dione

There total 4 articles about 9-Methyl-2-(p-tolylthio)acridine-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 244241-76-7
2-(2'-acetylphenylamino)-5-(4''-methylphenylthio)benzo[1,4]quinone

: 226260-32-8
2-(2'-methylphenylthio)-9-methyl-acridine[1,4]dione

Guidance literature:: With sulfuric acid; acetic acid; at 100 ℃; for 0.0833333h;
DOI:10.1080/00397919908086428

Reference yield:

: 5831-37-8
2-(p-tolylthio)cyclohexa-2,5-diene-1,4-dione

: 226260-32-8
2-(2'-methylphenylthio)-9-methyl-acridine[1,4]dione

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / CeCl₃*7H₂O / ethanol / 192 h / 20 °C

2: 97 percent / AcOH-H₂SO₄ / 0.08 h / 100 °C

With cerium(III) chloride; sulfuric acid; acetic acid; In ethanol; 1: Substitution / 2: Cyclization;
DOI:10.1080/00397919908086428

Reference yield:

: 106-45-6
para-thiocresol

: 226260-32-8
2-(2'-methylphenylthio)-9-methyl-acridine[1,4]dione

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / methanol / 0.08 h

2: 74 percent / CeCl₃*7H₂O / ethanol / 192 h / 20 °C

3: 97 percent / AcOH-H₂SO₄ / 0.08 h / 100 °C

With cerium(III) chloride; sulfuric acid; acetic acid; In methanol; ethanol; 1: Substitution / 2: Substitution / 3: Cyclization;
DOI:10.1080/00397919908086428