4,6-Dimethoxy-3-iod-salicylsaeuremethylester

Base Information

Chemical Name:4,6-Dimethoxy-3-iod-salicylsaeuremethylester
CAS No.:90794-41-5
Molecular Formula:C₁₀H₁₁IO₅
Molecular Weight:338.099
Hs Code.:

Synonyms:4,6-Dimethoxy-3-iod-salicylsaeuremethylester

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Chemical Property of 4,6-Dimethoxy-3-iod-salicylsaeuremethylester

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Technology Process of 4,6-Dimethoxy-3-iod-salicylsaeuremethylester

There total 3 articles about 4,6-Dimethoxy-3-iod-salicylsaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 51116-92-8
methyl 4,6-dimethoxysalicylate

: 90794-41-5
4,6-Dimethoxy-3-iod-salicylsaeuremethylester

Guidance literature:: With potassium iodate; iodine; In ethanol; water; at 28 ℃; for 14h; regioselective reaction;
DOI:10.1055/s-0035-1560434

Reference yield:

: 83-30-7
acide 2,4,6-trihydroxybenzoique

: 90794-41-5
4,6-Dimethoxy-3-iod-salicylsaeuremethylester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 15 h / 28 °C

2: iodine; potassium iodate / water; ethanol / 14 h / 28 °C

With potassium iodate; iodine; potassium carbonate; In ethanol; water; acetone;
DOI:10.1055/s-0035-1560434

Reference yield:

: 90794-41-5
4,6-Dimethoxy-3-iod-salicylsaeuremethylester

Guidance literature:: 4,6-Dimethoxy-salicylsaeuremethylester, Essigsaeure, konz. Schwefelsaeure, Iod, wfr. Iodwasserstoffsaeure;
DOI:10.1002/hlca.19620450658